3,5-dinitrobenzoic acid 4-(S)-isopropenyl-cyclohex-1-enylmethyl ester

Base Information

Chemical Name:3,5-dinitrobenzoic acid 4-(S)-isopropenyl-cyclohex-1-enylmethyl ester
CAS No.:1333393-09-1
Molecular Formula:C₁₇H₁₈N₂O₆
Molecular Weight:346.34
Hs Code.:

Synonyms:3,5-dinitrobenzoic acid 4-(S)-isopropenyl-cyclohex-1-enylmethyl ester

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Chemical Property of 3,5-dinitrobenzoic acid 4-(S)-isopropenyl-cyclohex-1-enylmethyl ester

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Technology Process of 3,5-dinitrobenzoic acid 4-(S)-isopropenyl-cyclohex-1-enylmethyl ester

There total 1 articles about 3,5-dinitrobenzoic acid 4-(S)-isopropenyl-cyclohex-1-enylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.2%

: 536-59-4,18457-55-1
(-)-perillyl alcohol

: 99-33-2
3,5-dinitrobenoyl chloride

: 1333393-09-1
3,5-dinitrobenzoic acid 4-(S)-isopropenyl-cyclohex-1-enylmethyl ester

Guidance literature:: (-)-perillyl alcohol; With triethylamine; In dichloromethane; at 15 - 20 ℃; for 0.75h;

3,5-dinitrobenoyl chloride; In dichloromethane; at 15 - 20 ℃; for 3.5h; Product distribution / selectivity;

Reference yield: 95.0%

: 1333393-09-1
3,5-dinitrobenzoic acid 4-(S)-isopropenyl-cyclohex-1-enylmethyl ester

: 536-59-4,18457-55-1
(-)-perillyl alcohol

Guidance literature:: With water; sodium hydroxide; In methanol; at 20 ℃; for 3.25h; Cooling with ice;

Reference yield:

: 1333393-09-1
3,5-dinitrobenzoic acid 4-(S)-isopropenyl-cyclohex-1-enylmethyl ester

: 1333393-11-5
4-chlorobenzoic acid 4(S)-isopropenyl cyclohex-1-enylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: water; sodium hydroxide / methanol / 3.25 h / 20 °C / Cooling with ice

2.1: triethylamine / dichloromethane / 0.75 h / 15 - 20 °C

2.2: 3.5 h / 15 - 20 °C

With water; triethylamine; sodium hydroxide; In methanol; dichloromethane;