pentafluorophenyl ester of N^α,N^G,N^G-tribenzyloxycarbonylarginyl0N^ε-benzyloxycarbonyllysine

Base Information

• Chemical Name: pentafluorophenyl ester of N^α,N^G,N^G-tribenzyloxycarbonylarginyl0N^ε-benzyloxycarbonyllysine
• CAS No.: 127290-79-3
• Molecular Formula: C₅₀H₄₉F₅N₆O₁₁
• Molecular Weight: 1004.96

Synonyms:pentafluorophenyl ester of N^α,N^G,N^G-tribenzyloxycarbonylarginyl0N^ε-benzyloxycarbonyllysine

Chemical Property of pentafluorophenyl ester of N^α,N^G,N^G-tribenzyloxycarbonylarginyl0N^ε-benzyloxycarbonyllysine

Chemical Property:

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Technology Process of pentafluorophenyl ester of N^α,N^G,N^G-tribenzyloxycarbonylarginyl0N^ε-benzyloxycarbonyllysine

There total 4 articles about pentafluorophenyl ester of N^α,N^G,N^G-tribenzyloxycarbonylarginyl0N^ε-benzyloxycarbonyllysine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

tris(carbobenzyloxy)-L-arginyl-Nε-(carbobenzyloxy)-L-lysine (80622-02-2) → pentafluorophenyl ester of Nα,NG,NG-tribenzyloxycarbonylarginyl0Nε-benzyloxycarbonyllysine (127290-79-3)

Guidance literature:

In 1,4-dioxane; at 20 ℃; for 2h;

Reference yield: 91.0%

tris(carbobenzyloxy)-L-arginyl-Nε-(carbobenzyloxy)-L-lysine (80622-02-2) → pentafluorophenyl ester of Nα,NG,NG-tribenzyloxycarbonylarginyl0Nε-benzyloxycarbonyllysine (127290-79-3)

Guidance literature:

Reference yield:

N6-[(benzyloxy)carbonyl]-L-lysine (1155-64-2,57705-97-2,67178-46-5,25931-47-9) → pentafluorophenyl ester of Nα,NG,NG-tribenzyloxycarbonylarginyl0Nε-benzyloxycarbonyllysine (127290-79-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent

2: 94 percent / dioxane / 2 h / 20 °C

In 1,4-dioxane; 1: Condensation / 2: Esterification;

upstream raw materials:

tris(carbobenzyloxy)-L-arginyl-N^ε-(carbobenzyloxy)-L-lysine

N₆-[(benzyloxy)carbonyl]-L-lysine

N^α,N^G,N^G-tri-Z-arginine p-nitrophenylester

Downstream raw materials:

H-L-Arg-L-Lys-L-Asp-L-Val-L-Tyr-OH*3HOAc

C₆₂H₇₃N₉O₁₇

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