5-Chloro-2-nitro-benzoic acid N-tert-butyl-N'-isopropylidene-hydrazide

Base Information

Chemical Name:5-Chloro-2-nitro-benzoic acid N-tert-butyl-N'-isopropylidene-hydrazide
CAS No.:182567-51-7
Molecular Formula:C₁₄H₁₈ClN₃O₃
Molecular Weight:311.768
Hs Code.:

Synonyms:5-Chloro-2-nitro-benzoic acid N-tert-butyl-N'-isopropylidene-hydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Chloro-2-nitro-benzoic acid N-tert-butyl-N'-isopropylidene-hydrazide

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Technology Process of 5-Chloro-2-nitro-benzoic acid N-tert-butyl-N'-isopropylidene-hydrazide

There total 1 articles about 5-Chloro-2-nitro-benzoic acid N-tert-butyl-N'-isopropylidene-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 33050-99-6
acetone tert-butylhydrazone

: 41994-44-9
5-chloro-2-nitrobenzoyl chloride

: 182567-51-7
5-Chloro-2-nitro-benzoic acid N-tert-butyl-N'-isopropylidene-hydrazide

Guidance literature:: With triethylamine; In tetrahydrofuran; toluene; Ambient temperature;
DOI:10.1002/jhet.5570330421

Reference yield: 92.0%

: 182567-51-7
5-Chloro-2-nitro-benzoic acid N-tert-butyl-N'-isopropylidene-hydrazide

: 182567-53-9
1-tert-butyl-(5-chloro-2-nitrobenzoyl)hydrazine

Guidance literature:: With hydrogenchloride; In ethanol; for 24h;
DOI:10.1002/jhet.5570330421

Reference yield:

: 182567-51-7
5-Chloro-2-nitro-benzoic acid N-tert-butyl-N'-isopropylidene-hydrazide

: 182567-55-1
1-tert-butyl-(2-amino-5-chlorobenzoyl)hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 10percent HCl / ethanol / 24 h

2: 75 percent / H₂ / 5percent Pt/C / ethanol / 2 h / 2585.7 Torr

With hydrogenchloride; hydrogen; platinum on activated charcoal; In ethanol;
DOI:10.1002/jhet.5570330421