N-methyl-O-(4-(2-perfluoroctylethyl)benzyl)hydroxylamine hydrochloride

Base Information

Chemical Name:N-methyl-O-(4-(2-perfluoroctylethyl)benzyl)hydroxylamine hydrochloride
CAS No.:1313585-54-4
Molecular Formula:C₁₈H₁₄F₁₇NO*ClH
Molecular Weight:619.749
Hs Code.:

Synonyms:N-methyl-O-(4-(2-perfluoroctylethyl)benzyl)hydroxylamine hydrochloride

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Chemical Property of N-methyl-O-(4-(2-perfluoroctylethyl)benzyl)hydroxylamine hydrochloride

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Technology Process of N-methyl-O-(4-(2-perfluoroctylethyl)benzyl)hydroxylamine hydrochloride

There total 4 articles about N-methyl-O-(4-(2-perfluoroctylethyl)benzyl)hydroxylamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1313585-46-4
tert-butyl methyl(4-(2-perfluoroctylethyl)benzyloxy)carbamate

: 1313585-54-4
N-methyl-O-(4-(2-perfluoroctylethyl)benzyl)hydroxylamine hydrochloride

Guidance literature:: With ethanol; acetyl chloride; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tet.2011.05.039

Reference yield:

: 1-(bromomethyl)-4-(3,3,4,4,5,5,6,6,7,7,8,8,9,9,10,10,10-heptadecafluorodecyl)benzene

: 1313585-54-4
N-methyl-O-(4-(2-perfluoroctylethyl)benzyl)hydroxylamine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / -5 - 20 °C / Inert atmosphere; Darkness

2: caesium carbonate / acetonitrile / 3 h / 45 °C

3: ethanol; acetyl chloride / 16 h / 20 °C / Inert atmosphere

With ethanol; caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; acetyl chloride; In tetrahydrofuran; acetonitrile;
DOI:10.1016/j.tet.2011.05.039

Reference yield:

: 1313585-45-3
tert-butyl 4-(2-perfluoroctylethyl)benzyloxycarbamate

: 1313585-54-4
N-methyl-O-(4-(2-perfluoroctylethyl)benzyl)hydroxylamine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: caesium carbonate / acetonitrile / 3 h / 45 °C

2: ethanol; acetyl chloride / 16 h / 20 °C / Inert atmosphere

With ethanol; caesium carbonate; acetyl chloride; In acetonitrile;
DOI:10.1016/j.tet.2011.05.039