dicarbonyl{1-4-η-1-(methoxycarbonyl)-5-hydroxycyclohepta-1,3-dienyl}(triphenyl phosphite)iron

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Chemical Name:dicarbonyl{1-4-η-1-(methoxycarbonyl)-5-hydroxycyclohepta-1,3-dienyl}(triphenyl phosphite)iron
CAS No.:137203-86-2
Molecular Formula:C₂₉H₂₇FeO₈P
Molecular Weight:590.349
Hs Code.:

Synonyms:dicarbonyl{1-4-η-1-(methoxycarbonyl)-5-hydroxycyclohepta-1,3-dienyl}(triphenyl phosphite)iron

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Chemical Property of dicarbonyl{1-4-η-1-(methoxycarbonyl)-5-hydroxycyclohepta-1,3-dienyl}(triphenyl phosphite)iron

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Technology Process of dicarbonyl{1-4-η-1-(methoxycarbonyl)-5-hydroxycyclohepta-1,3-dienyl}(triphenyl phosphite)iron

There total 1 articles about dicarbonyl{1-4-η-1-(methoxycarbonyl)-5-hydroxycyclohepta-1,3-dienyl}(triphenyl phosphite)iron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 137203-94-2
dicarbonyl{1-5-η-1-(methoxycarbonyl)cyclohepta-1,3-dienylium}(triphenyl phosphite)iron hexafluorophosphate

: 137203-86-2
dicarbonyl{1-4-η-1-(methoxycarbonyl)-5-hydroxycyclohepta-1,3-dienyl}(triphenyl phosphite)iron

Guidance literature:: With NaOH; In tetrahydrofuran; (Ar or N2); addn. of aq. NaOH to soln. of Fe complex, 0°C, stirring, 30 min; warming to room temp., extn. with Et2O three times, washing with brine, drying (MgSO4), removal of solvent in vac., flash chromy. (SiO2, 50% EtOAc/hexanes);
DOI:10.1021/om00037a072