C₁₈H₁₈Cl₂O₂

Base Information

Chemical Name:C₁₈H₁₈Cl₂O₂
CAS No.:1415596-71-2
Molecular Formula:C₁₈H₁₈Cl₂O₂
Molecular Weight:337.246
Hs Code.:

C<sub>18</sub>H<sub>18</sub>Cl<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₈H₁₈Cl₂O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₈H₁₈Cl₂O₂

Chemical Property:

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Technology Process of C₁₈H₁₈Cl₂O₂

There total 6 articles about C₁₈H₁₈Cl₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1415596-70-1
C₁₈H₁₉ClO₂

: 1415596-71-2
C₁₈H₁₈Cl₂O₂

Guidance literature:: With sulfuryl dichloride; In dichloromethane; at -10 ℃;
DOI:10.1016/j.bmcl.2012.10.022

Reference yield:

: 41841-16-1
(4-bromo-phenyl)-acetic acid methyl ester

: 1415596-71-2
C₁₈H₁₈Cl₂O₂

Guidance literature:: Multi-step reaction with 6 steps

1: copper(I) oxide; caesium carbonate / N,N-dimethyl-formamide / 110 °C / Molecular sieve

2: sodium hydroxide / methanol / Reflux

3: thionyl chloride / Reflux

4: triethylamine / dichloromethane / 0 °C

5: tetrahydrofuran / -78 °C

6: sulfuryl dichloride / dichloromethane / -10 °C

With copper(I) oxide; thionyl chloride; sulfuryl dichloride; caesium carbonate; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.10.022

Reference yield:

: 69383-41-1
methyl 2-(4-(4-chlorophenoxy)phenyl)acetate

: 1415596-71-2
C₁₈H₁₈Cl₂O₂

Guidance literature:: Multi-step reaction with 5 steps

1: sodium hydroxide / methanol / Reflux

2: thionyl chloride / Reflux

3: triethylamine / dichloromethane / 0 °C

4: tetrahydrofuran / -78 °C

5: sulfuryl dichloride / dichloromethane / -10 °C

With thionyl chloride; sulfuryl dichloride; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2012.10.022