C₂₈H₄₀O₆

Base Information

Chemical Name:C₂₈H₄₀O₆
CAS No.:939378-66-2
Molecular Formula:C₂₈H₄₀O₆
Molecular Weight:472.622
Hs Code.:

C<sub>28</sub>H<sub>40</sub>O<sub>6</sub>

Synonyms:C₂₈H₄₀O₆

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Chemical Property of C₂₈H₄₀O₆

Chemical Property:

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Technology Process of C₂₈H₄₀O₆

There total 5 articles about C₂₈H₄₀O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 939378-82-2
C₃₄H₅₂O₆Si

: 939378-66-2
C₂₈H₄₀O₆

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / NaBH₄; (H₂NCH₂)2; H₂ / Ni(OAc)2 / ethanol / 5 h / 23 °C / 760.05 Torr

2: 70 percent / n-Bu₄NF / tetrahydrofuran / 12 h / 23 °C

With sodium tetrahydroborate; tetrabutyl ammonium fluoride; hydrogen; ethylenediamine; nickel diacetate; In tetrahydrofuran; ethanol;
DOI:10.1016/j.bmcl.2007.01.096

Reference yield:

: 939378-81-1
C₂₉H₄₂O₆Si

: 939378-66-2
C₂₈H₄₀O₆

Guidance literature:: Multi-step reaction with 5 steps

1: OsO₄; NMO / 2-methyl-propan-2-ol / 12 h / 23 °C

2: NaIO₄/SiO₂ / CH₂Cl₂ / 1.5 h / 23 °C

3: NaN(SiMe₃)2 / toluene; tetrahydrofuran / -90 - 23 °C

4: 85 percent / NaBH₄; (H₂NCH₂)2; H₂ / Ni(OAc)2 / ethanol / 5 h / 23 °C / 760.05 Torr

5: 70 percent / n-Bu₄NF / tetrahydrofuran / 12 h / 23 °C

With sodium tetrahydroborate; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; tetrabutyl ammonium fluoride; hydrogen; sodium hexamethyldisilazane; silica gel; ethylenediamine; nickel diacetate; In tetrahydrofuran; ethanol; dichloromethane; toluene; tert-butyl alcohol; 3: Wittig olefination;
DOI:10.1016/j.bmcl.2007.01.096

Reference yield:

: C₂₉H₄₄O₈Si

: 939378-66-2
C₂₈H₄₀O₆

Guidance literature:: Multi-step reaction with 4 steps

1: NaIO₄/SiO₂ / CH₂Cl₂ / 1.5 h / 23 °C

2: NaN(SiMe₃)2 / toluene; tetrahydrofuran / -90 - 23 °C

3: 85 percent / NaBH₄; (H₂NCH₂)2; H₂ / Ni(OAc)2 / ethanol / 5 h / 23 °C / 760.05 Torr

4: 70 percent / n-Bu₄NF / tetrahydrofuran / 12 h / 23 °C

With sodium tetrahydroborate; sodium periodate; tetrabutyl ammonium fluoride; hydrogen; sodium hexamethyldisilazane; silica gel; ethylenediamine; nickel diacetate; In tetrahydrofuran; ethanol; dichloromethane; toluene; 2: Wittig olefination;
DOI:10.1016/j.bmcl.2007.01.096