Technology Process of C24H28Br2O2
There total 3 articles about C24H28Br2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 2.) LAH / 1.) PhCH3, heating, 2.) THF, reflux
2: 98 percent / KH / tetrahydrofuran
3: 1.) cupric bromide, propylene oxide, bromine, 2.) bromine / 1.) CCl4, THF, -78 deg C, 15 min, to 0 deg C, 15 min, 2.) CCl4, -78 deg C, 15 min, to 0 deg C, 15 min
With
lithium aluminium tetrahydride; bromine; potassium hydride; methyloxirane; copper(ll) bromide;
In
tetrahydrofuran;
DOI:10.1021/ja00360a057
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 98 percent / KH / tetrahydrofuran
2: 1.) cupric bromide, propylene oxide, bromine, 2.) bromine / 1.) CCl4, THF, -78 deg C, 15 min, to 0 deg C, 15 min, 2.) CCl4, -78 deg C, 15 min, to 0 deg C, 15 min
With
bromine; potassium hydride; methyloxirane; copper(ll) bromide;
In
tetrahydrofuran;
DOI:10.1021/ja00360a057
- Guidance literature:
-
With
bromine; methyloxirane; copper(ll) bromide;
Yield given. Multistep reaction;
1.) CCl4, THF, -78 deg C, 15 min, to 0 deg C, 15 min, 2.) CCl4, -78 deg C, 15 min, to 0 deg C, 15 min;
DOI:10.1021/ja00360a057