4-methyl-N-(4-methylbenzyl)-N'-(4-methylbenzylidene)benzenesulfonohydrazide

Base Information

Chemical Name:4-methyl-N-(4-methylbenzyl)-N'-(4-methylbenzylidene)benzenesulfonohydrazide
CAS No.:1430811-53-2
Molecular Formula:C₂₃H₂₄N₂O₂S
Molecular Weight:392.522
Hs Code.:

Synonyms:4-methyl-N-(4-methylbenzyl)-N'-(4-methylbenzylidene)benzenesulfonohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methyl-N-(4-methylbenzyl)-N'-(4-methylbenzylidene)benzenesulfonohydrazide

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Technology Process of 4-methyl-N-(4-methylbenzyl)-N'-(4-methylbenzylidene)benzenesulfonohydrazide

There total 3 articles about 4-methyl-N-(4-methylbenzyl)-N'-(4-methylbenzylidene)benzenesulfonohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 40739-81-9
p-tolualdehyde p-toluenesulfonylhydrazone

: 1430811-53-2
4-methyl-N-(4-methylbenzyl)-N'-(4-methylbenzylidene)benzenesulfonohydrazide

Guidance literature:: With potassium carbonate; In nitromethane; at 90 ℃; for 3h; Schlenk technique;
DOI:10.1016/j.tet.2013.03.055

Reference yield: 48.0%

: 40739-81-9
p-tolualdehyde p-toluenesulfonylhydrazone

: 1430811-53-2
4-methyl-N-(4-methylbenzyl)-N'-(4-methylbenzylidene)benzenesulfonohydrazide

: 52209-08-2
4-methylbenzyl 4-methylbenzenesulfinate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In nitromethane; at 90 ℃; for 2h;
DOI:10.1055/s-0039-1690754

Reference yield:

: 104-87-0
4-methyl-benzaldehyde

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1430811-53-2
4-methyl-N-(4-methylbenzyl)-N'-(4-methylbenzylidene)benzenesulfonohydrazide

: 52209-08-2
4-methylbenzyl 4-methylbenzenesulfinate

Guidance literature:: Multi-step reaction with 2 steps

1: nitromethane / 2 h / 25 °C

2: N-ethyl-N,N-diisopropylamine / nitromethane / 2 h / 90 °C

With N-ethyl-N,N-diisopropylamine; In nitromethane;
DOI:10.1055/s-0039-1690754