(2S)-2-hydroxy-2-(2-hydroxy-4-tert-butylphenyl)propanoic acid (-)-menthyl ester

Base Information

Chemical Name:(2S)-2-hydroxy-2-(2-hydroxy-4-tert-butylphenyl)propanoic acid (-)-menthyl ester
CAS No.:100993-14-4
Molecular Formula:C₂₃H₃₆O₄
Molecular Weight:376.536
Hs Code.:

Synonyms:(2S)-2-hydroxy-2-(2-hydroxy-4-tert-butylphenyl)propanoic acid (-)-menthyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S)-2-hydroxy-2-(2-hydroxy-4-tert-butylphenyl)propanoic acid (-)-menthyl ester

Chemical Property:

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Technology Process of (2S)-2-hydroxy-2-(2-hydroxy-4-tert-butylphenyl)propanoic acid (-)-menthyl ester

There total 5 articles about (2S)-2-hydroxy-2-(2-hydroxy-4-tert-butylphenyl)propanoic acid (-)-menthyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 585-34-2
3-tert-butylphenyol

: 951-98-4,53651-68-6,60661-55-4,93059-38-2
(+)-menthyl pyruvate

: 100990-39-4,100990-40-7,100993-14-4,100993-15-5
menthyl (+)-(2R)-(2-hydroxy-4-tert-butylphenyl)lactate

: 100990-39-4,100990-40-7,100993-14-4,100993-15-5
C₂₃H₃₆O₄

Guidance literature:: (+)-menthylOTiCl₃; In dichloromethane; at -60 ℃; for 5h; Yields of byproduct given;
DOI:10.1016/S0040-4039(00)98370-9

Reference yield: 67.0%

: 585-34-2
3-tert-butylphenyol

: 951-98-4,53651-68-6,60661-55-4,93059-38-2
(+)-menthyl pyruvate

: 100990-39-4,100990-40-7,100993-14-4,100993-15-5
menthyl (+)-(2R)-(2-hydroxy-4-tert-butylphenyl)lactate

: 100990-39-4,100990-40-7,100993-14-4,100993-15-5
C₂₃H₃₆O₄

Guidance literature:: (+)-menthylOTiCl₃; In dichloromethane; at -60 ℃; for 5h; Yields of byproduct given;
DOI:10.1016/S0040-4039(00)98370-9

Reference yield: 58.0%

: 585-34-2
3-tert-butylphenyol

: 951-98-4
2-Oxo-propionic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

: 100990-39-4,100990-40-7,100993-14-4,100993-15-5
2-(4-tert-Butyl-2-hydroxy-phenyl)-2-hydroxy-propionic acid (1R,2S,5R)-2-isopropyl-5-methyl-cyclohexyl ester

: 100990-39-4,100990-40-7,100993-14-4,100993-15-5
menthyl (-)-(2S)-(2-hydroxy-4-tert-butylphenyl)lactate

Guidance literature:: (+)-menthylO(Et)AlCl; In hexane; dichloromethane; at -20 ℃; for 24h; Yields of byproduct given;
DOI:10.1016/S0040-4039(00)98370-9