1,3-dibenzoyladamantane dihydrazone

Base Information

• Chemical Name: 1,3-dibenzoyladamantane dihydrazone
• CAS No.: 1036278-86-0
• Molecular Formula: C₂₄H₂₈N₄
• Molecular Weight: 372.513

Synonyms:1,3-dibenzoyladamantane dihydrazone

Chemical Property of 1,3-dibenzoyladamantane dihydrazone

Chemical Property:

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Technology Process of 1,3-dibenzoyladamantane dihydrazone

There total 1 articles about 1,3-dibenzoyladamantane dihydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.4%

1,3-dibenzoyldadamantane (167902-36-5) → 1-(phenylcarbinol)-3-benzoyladamantane hydrazone (1036278-88-2) + 1,3-dibenzoyladamantane dihydrazone (1036278-86-0)

Guidance literature:

With hydrazine hydrate; In ethanol; for 96h; Heating;

DOI:10.1002/poc.1319

Reference yield: 98.2%

1,3-dibenzoyladamantane dihydrazone (1036278-86-0) → 1,3-bis(diazobenzyl)adamantane (1036278-85-9)

Guidance literature:

With barium permanganate; calcium oxide; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1002/poc.1319

Reference yield: 65.0%

1,3-dibenzoyladamantane dihydrazone (1036278-86-0) + 1,3-dibenzoyldadamantane (167902-36-5) → C48H48N4 (1036278-87-1)

Guidance literature:

With toluene-4-sulfonic acid; In xylene; for 3h; Heating;

DOI:10.1002/poc.1319

upstream raw materials:

1,3-dibenzoyldadamantane

Downstream raw materials:

1,3-bis(diazobenzyl)adamantane

C₄₈H₄₈N₄

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