C₃₃H₄₅N₅O₆S₂

Base Information

Chemical Name:C₃₃H₄₅N₅O₆S₂
CAS No.:164412-84-4
Molecular Formula:C₃₃H₄₅N₅O₆S₂
Molecular Weight:671.882
Hs Code.:

C<sub>33</sub>H<sub>45</sub>N<sub>5</sub>O<sub>6</sub>S<sub>2</sub>

Synonyms:C₃₃H₄₅N₅O₆S₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₄₅N₅O₆S₂

Chemical Property:

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Technology Process of C₃₃H₄₅N₅O₆S₂

There total 12 articles about C₃₃H₄₅N₅O₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5720-05-8
4-methylphenylboronic acid

: 164412-84-4
C₃₃H₄₅N₅O₆S₂

Guidance literature:: Multi-step reaction with 7 steps

1: 93 percent / aq. Na₂CO₃, triphenylphosphine, palladium acetate / ethanol; toluene / 4 h / Heating

2: 64 percent / N-bromosuccinimide, benzoyl peroxide / chlorobenzene / 1 h / 120 °C

3: K₂CO₃ / dimethylformamide / 45 h / 20 - 25 °C

4: 81 percent / conc. HCl / ethanol / 2 h / Heating

5: 62 percent / 2N NaOH / ethanol / 36 h / Ambient temperature

6: 51 percent / 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride / ethyl acetate / 16 h / Ambient temperature

7: 1.) K₂CO₃ / 1.) DME, RT, 30 min, 2.) DME, reflux, 1 h

With hydrogenchloride; sodium hydroxide; N-Bromosuccinimide; Perbenzoic acid; palladium diacetate; sodium carbonate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; In ethanol; ethyl acetate; N,N-dimethyl-formamide; chlorobenzene; toluene;
DOI:10.1021/jm00013a013

Reference yield:

: 92748-09-9
2-bromobenzene-1-sulfonamide

: 164412-84-4
C₃₃H₄₅N₅O₆S₂

Guidance literature:: Multi-step reaction with 8 steps

1: 98 percent / dimethylformamide / 2 h / Ambient temperature

2: 93 percent / aq. Na₂CO₃, triphenylphosphine, palladium acetate / ethanol; toluene / 4 h / Heating

3: 64 percent / N-bromosuccinimide, benzoyl peroxide / chlorobenzene / 1 h / 120 °C

4: K₂CO₃ / dimethylformamide / 45 h / 20 - 25 °C

5: 81 percent / conc. HCl / ethanol / 2 h / Heating

6: 62 percent / 2N NaOH / ethanol / 36 h / Ambient temperature

7: 51 percent / 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride / ethyl acetate / 16 h / Ambient temperature

8: 1.) K₂CO₃ / 1.) DME, RT, 30 min, 2.) DME, reflux, 1 h

With hydrogenchloride; sodium hydroxide; N-Bromosuccinimide; Perbenzoic acid; palladium diacetate; sodium carbonate; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; In ethanol; ethyl acetate; N,N-dimethyl-formamide; chlorobenzene; toluene;
DOI:10.1021/jm00013a013

Reference yield:

: 638-29-9
n-valeryl chloride

: 164412-84-4
C₃₃H₄₅N₅O₆S₂

Guidance literature:: Multi-step reaction with 8 steps

1: 75 percent / pyridine / CH₂Cl₂ / 0 °C

2: 87 percent / triethylamine / ethanol / 50 h / 0 °C

3: 72 percent / PCl₅, 4-(dimethylamino)pyridine / CH₂Cl₂ / 12 h / Ambient temperature

4: K₂CO₃ / dimethylformamide / 45 h / 20 - 25 °C

5: 81 percent / conc. HCl / ethanol / 2 h / Heating

6: 62 percent / 2N NaOH / ethanol / 36 h / Ambient temperature

7: 51 percent / 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride / ethyl acetate / 16 h / Ambient temperature

8: 1.) K₂CO₃ / 1.) DME, RT, 30 min, 2.) DME, reflux, 1 h

With pyridine; hydrogenchloride; dmap; sodium hydroxide; phosphorus pentachloride; potassium carbonate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm00013a013