methyl 2-acetamido-6-O-benzyl-2-N,3-O-carbonyl-2-deoxy-[2,3,4,6-O-benzyl-α-D-glucopyranosyl]-(1->4)-α-D-glucopyranoside

Base Information

Chemical Name:methyl 2-acetamido-6-O-benzyl-2-N,3-O-carbonyl-2-deoxy-[2,3,4,6-O-benzyl-α-D-glucopyranosyl]-(1->4)-α-D-glucopyranoside
CAS No.:526199-58-6
Molecular Formula:C₅₁H₅₅NO₁₂
Molecular Weight:873.997
Hs Code.:

Synonyms:methyl 2-acetamido-6-O-benzyl-2-N,3-O-carbonyl-2-deoxy-[2,3,4,6-O-benzyl-α-D-glucopyranosyl]-(1->4)-α-D-glucopyranoside

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Chemical Property of methyl 2-acetamido-6-O-benzyl-2-N,3-O-carbonyl-2-deoxy-[2,3,4,6-O-benzyl-α-D-glucopyranosyl]-(1->4)-α-D-glucopyranoside

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Technology Process of methyl 2-acetamido-6-O-benzyl-2-N,3-O-carbonyl-2-deoxy-[2,3,4,6-O-benzyl-α-D-glucopyranosyl]-(1->4)-α-D-glucopyranoside

There total 12 articles about methyl 2-acetamido-6-O-benzyl-2-N,3-O-carbonyl-2-deoxy-[2,3,4,6-O-benzyl-α-D-glucopyranosyl]-(1->4)-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 74808-09-6
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl trichloroacetimidate

: 526199-44-0
methyl 2-acetamido-6-O-benzyl-2-N,3-O-carbonyl-2-deoxy-α-D-glucopyranoside

: methyl 2-acetamido-6-O-benzyl-2-N,3-O-carbonyl-2-deoxy-[2,3,4,6-O-benzyl-β-D-glucopyranosyl]-(1->4)-α-D-glucopyranoside

: 526199-58-6
methyl 2-acetamido-6-O-benzyl-2-N,3-O-carbonyl-2-deoxy-[2,3,4,6-O-benzyl-α-D-glucopyranosyl]-(1->4)-α-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 - 0 ℃; for 1.5h;
DOI:10.1021/ol0342305

Reference yield: 63.0%

: 117307-17-2
phenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-glucopyranoside sulfoxide

: 526199-44-0
methyl 2-acetamido-6-O-benzyl-2-N,3-O-carbonyl-2-deoxy-α-D-glucopyranoside

: 526199-58-6
methyl 2-acetamido-6-O-benzyl-2-N,3-O-carbonyl-2-deoxy-[2,3,4,6-O-benzyl-α-D-glucopyranosyl]-(1->4)-α-D-glucopyranoside

Guidance literature:: phenyl 2,3,4,6-tetra-O-benzyl-1-thio-β-D-glucopyranoside sulfoxide; With trifluoromethylsulfonic anhydride; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -60 ℃; for 0.166667h;

methyl 2-acetamido-6-O-benzyl-2-N,3-O-carbonyl-2-deoxy-α-D-glucopyranoside; In dichloromethane; at -60 ℃; for 2h;
DOI:10.1021/ol0342305

Reference yield: 63.0%

: 157087-54-2
phenyl 2,3,4,6-tetra-O-benzyl-1-thio-α-D-glucopyranoside sulfoxide

: 526199-44-0
methyl 2-acetamido-6-O-benzyl-2-N,3-O-carbonyl-2-deoxy-α-D-glucopyranoside

: 526199-58-6
methyl 2-acetamido-6-O-benzyl-2-N,3-O-carbonyl-2-deoxy-[2,3,4,6-O-benzyl-α-D-glucopyranosyl]-(1->4)-α-D-glucopyranoside

Guidance literature:: With trifluoromethanesulfonic acid anhydride; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -60 - 0 ℃;
DOI:10.1021/jo0482559