C₃₉H₄₈O₆Si

Base Information

Chemical Name:C₃₉H₄₈O₆Si
CAS No.:1354973-46-8
Molecular Formula:C₃₉H₄₈O₆Si
Molecular Weight:640.892
Hs Code.:

C<sub>39</sub>H<sub>48</sub>O<sub>6</sub>Si

Synonyms:C₃₉H₄₈O₆Si

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Chemical Property of C₃₉H₄₈O₆Si

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Technology Process of C₃₉H₄₈O₆Si

There total 11 articles about C₃₉H₄₈O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1338989-57-3
C₂₃H₃₀O₆

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1354973-46-8
C₃₉H₄₈O₆Si

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 24 ℃;
DOI:10.1016/j.tetlet.2011.08.051

Reference yield:

: C₁₁H₁₂O₄

: 1354973-46-8
C₃₉H₄₈O₆Si

Guidance literature:: Multi-step reaction with 8 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 25 °C

2: tert.-butyl lithium / tetrahydrofuran / -78 °C

3: zinc(II) tetrahydroborate / diethyl ether / -78 - -30 °C

4: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 0 - 24 °C

5: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 0 - 24 °C

6: tetrabutyl ammonium fluoride / tetrahydrofuran / 25 °C

7: lithium aluminium tetrahydride / tetrahydrofuran / -15 °C

8: 1H-imidazole / N,N-dimethyl-formamide / 24 °C

With 1H-imidazole; tert.-butylhydroperoxide; dmap; lithium aluminium tetrahydride; zinc(II) tetrahydroborate; bis(acetylacetonate)oxovanadium; tetrabutyl ammonium fluoride; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2011.08.051

Reference yield:

: 1338989-47-1
C₁₃H₁₇NO₄

: 1354973-46-8
C₃₉H₄₈O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1: tert.-butyl lithium / tetrahydrofuran / -78 °C

2: zinc(II) tetrahydroborate / diethyl ether / -78 - -30 °C

3: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 0 - 24 °C

4: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 0 - 24 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 25 °C

6: lithium aluminium tetrahydride / tetrahydrofuran / -15 °C

7: 1H-imidazole / N,N-dimethyl-formamide / 24 °C

With 1H-imidazole; tert.-butylhydroperoxide; lithium aluminium tetrahydride; zinc(II) tetrahydroborate; bis(acetylacetonate)oxovanadium; tetrabutyl ammonium fluoride; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2011.08.051