<(2R)-(2α,4aβ,5β,6α,7aβ)>-hexahydro-5-(methoxymethyl)-2-phenyl-6-(phenylmethoxy)cyclopenta-1,3-dioxin

Base Information

Chemical Name:<(2R)-(2α,4aβ,5β,6α,7aβ)>-hexahydro-5-(methoxymethyl)-2-phenyl-6-(phenylmethoxy)cyclopenta-1,3-dioxin
CAS No.:106139-77-9
Molecular Formula:C₂₂H₂₆O₄
Molecular Weight:354.446
Hs Code.:

Synonyms:<(2R)-(2α,4aβ,5β,6α,7aβ)>-hexahydro-5-(methoxymethyl)-2-phenyl-6-(phenylmethoxy)cyclopenta-1,3-dioxin

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Chemical Property of <(2R)-(2α,4aβ,5β,6α,7aβ)>-hexahydro-5-(methoxymethyl)-2-phenyl-6-(phenylmethoxy)cyclopenta-1,3-dioxin

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Technology Process of <(2R)-(2α,4aβ,5β,6α,7aβ)>-hexahydro-5-(methoxymethyl)-2-phenyl-6-(phenylmethoxy)cyclopenta-1,3-dioxin

There total 2 articles about <(2R)-(2α,4aβ,5β,6α,7aβ)>-hexahydro-5-(methoxymethyl)-2-phenyl-6-(phenylmethoxy)cyclopenta-1,3-dioxin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115859-28-4,116002-03-0
Imidazole-1-carbothioic acid O-[(2R,4S,5R)-4-((Z)-(R)-2-benzyloxy-4-methoxy-but-3-enyl)-2-phenyl-[1,3]dioxan-5-yl] ester

: 106139-77-9
<(2R)-(2α,4aβ,5β,6α,7aβ)>-hexahydro-5-(methoxymethyl)-2-phenyl-6-(phenylmethoxy)cyclopenta-1,3-dioxin

Guidance literature:: With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 2h; Yield given; Heating;
DOI:10.1021/jo00254a020

Reference yield:

: 115859-27-3,115938-45-9
2,4-dideoxy-1-O-methyl-3-(phenylmethyl)-5,7-O-(phenylmethylene)-D-ribo-hept-1-enitol

: 106139-77-9
<(2R)-(2α,4aβ,5β,6α,7aβ)>-hexahydro-5-(methoxymethyl)-2-phenyl-6-(phenylmethoxy)cyclopenta-1,3-dioxin

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / 1,2-dichloro-ethane / 3 h / Heating

2: Bu₃SnH, AIBN / toluene / 2 h / Heating

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In 1,2-dichloro-ethane; toluene;
DOI:10.1021/jo00254a020

Reference yield: 65.0%

: 106139-77-9
<(2R)-(2α,4aβ,5β,6α,7aβ)>-hexahydro-5-(methoxymethyl)-2-phenyl-6-(phenylmethoxy)cyclopenta-1,3-dioxin

: 115859-29-5
<1S-(1α,2α,3β,4α)>-3-(methoxymethyl)-4-(phenylmethoxy)-2-<(phenylmethoxy)methyl>cyclopentanol

: 115859-30-8
<1S-(1α,2β,3α,5α)>-2-(methoxymethyl)-3,5-bis(phenylmethoxy)cyclopentanemethanol

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether; dichloromethane; for 1h; Ambient temperature;
DOI:10.1021/jo00254a020