(Z)-toluene-4-sulfonic acid 5-(tert-butyl-dimethyl-silanyloxy)-3-phenyl-pent-4-enyl ester

Base Information

Chemical Name:(Z)-toluene-4-sulfonic acid 5-(tert-butyl-dimethyl-silanyloxy)-3-phenyl-pent-4-enyl ester
CAS No.:1206146-61-3
Molecular Formula:C₂₄H₃₄O₄SSi
Molecular Weight:446.683
Hs Code.:

Synonyms:(Z)-toluene-4-sulfonic acid 5-(tert-butyl-dimethyl-silanyloxy)-3-phenyl-pent-4-enyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-toluene-4-sulfonic acid 5-(tert-butyl-dimethyl-silanyloxy)-3-phenyl-pent-4-enyl ester

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Technology Process of (Z)-toluene-4-sulfonic acid 5-(tert-butyl-dimethyl-silanyloxy)-3-phenyl-pent-4-enyl ester

There total 1 articles about (Z)-toluene-4-sulfonic acid 5-(tert-butyl-dimethyl-silanyloxy)-3-phenyl-pent-4-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1076691-75-2
5-oxo-3-phenylpentyl 4-methylbenzenesulfonate

: 69739-34-0
t-butyldimethylsiyl triflate

: 1206146-61-3
(Z)-toluene-4-sulfonic acid 5-(tert-butyl-dimethyl-silanyloxy)-3-phenyl-pent-4-enyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 ℃; for 3.08333h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jo902426z

Reference yield: 82.0%

: 1206146-61-3
(Z)-toluene-4-sulfonic acid 5-(tert-butyl-dimethyl-silanyloxy)-3-phenyl-pent-4-enyl ester

: 1206146-63-5
(Z)-(5-azido-3-phenyl-pent-1-enyloxy)-tert-butyl-dimethyl-silane

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 50 ℃; for 10h; Inert atmosphere;
DOI:10.1021/jo902426z DOI:10.1055/s-0030-1259062