9-(2-hydroxylmethylphenyl)-3,6-bis(diethylamino)-xanthylium chloride

Base Information

• Chemical Name: 9-(2-hydroxylmethylphenyl)-3,6-bis(diethylamino)-xanthylium chloride
• CAS No.: 1235977-21-5
• Molecular Formula: C₂₈H₃₃N₂O₂*Cl
• Molecular Weight: 465.035
• Mol file: 1235977-21-5.mol

Synonyms:9-(2-hydroxylmethylphenyl)-3,6-bis(diethylamino)-xanthylium chloride

Chemical Property of 9-(2-hydroxylmethylphenyl)-3,6-bis(diethylamino)-xanthylium chloride

Chemical Property:

Purity/Quality:

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Technology Process of 9-(2-hydroxylmethylphenyl)-3,6-bis(diethylamino)-xanthylium chloride

There total 5 articles about 9-(2-hydroxylmethylphenyl)-3,6-bis(diethylamino)-xanthylium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

rhodamine B (39393-39-0) → 9-(2-hydroxylmethylphenyl)-3,6-bis(diethylamino)-xanthylium chloride (1235977-21-5)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 12h; Inert atmosphere; Cooling with ice;

Reference yield: 66.0%

N-(9-(2-(((4-(4-(bis(2-chloroethyl)amino)phenyl)butanoyl)oxy)methyl)phenyl)-6-(diethylamino)-3H-xanthen-3-ylidene)-N-ethylethanaminium chloride → 9-(2-hydroxylmethylphenyl)-3,6-bis(diethylamino)-xanthylium chloride (1235977-21-5)

Guidance literature:

In water; acetonitrile; Irradiation;

DOI:10.1039/d0cc03524f

Reference yield: 54.0%

rhodamine B (81-88-9) → 9-(2-hydroxylmethylphenyl)-3,6-bis(diethylamino)-xanthylium chloride (1235977-21-5)

Guidance literature:

rhodamine B; With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

With sulfur; at 160 ℃; for 0.5h; Vacuum;

With hydrogenchloride; In ethanol; water; at 20 ℃;

DOI:10.1021/ol1011967

upstream raw materials:

rhodamine B

rhodamine B

Downstream raw materials:

9-(2-bromomethylphenyl)-3,6-bis(diethylamino)-xanthylium chloride