N-(methylcarbamoyl)homotyrosine methyl ester

Base Information

Chemical Name:N-(methylcarbamoyl)homotyrosine methyl ester
CAS No.:110936-12-4
Molecular Formula:C₁₃H₁₇NO₅
Molecular Weight:267.282
Hs Code.:

Synonyms:N-(methylcarbamoyl)homotyrosine methyl ester

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Chemical Property of N-(methylcarbamoyl)homotyrosine methyl ester

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of N-(methylcarbamoyl)homotyrosine methyl ester

There total 4 articles about N-(methylcarbamoyl)homotyrosine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 110971-27-2
(2Z)-2-<(methoxycarbonyl)amino>-4-(4-methoxyphenyl)but-2-enoic acid

: 110936-12-4
N-(methylcarbamoyl)homotyrosine methyl ester

: 110936-09-9
(2R)-2-<(methoxycarbonyl)amino>-4-(4-methoxyphenyl)-butanoic acid

Guidance literature:: With [Rh(bicyclo[2.2.1]hepta-2,5-diene)((2S,3S)-(-)-2,3-bis(diphenylphosphino)butane)]ClO₄; hydrogen; sodium acetate; In methanol; at 20 ℃; for 96h; under 2068.6 Torr; Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00232a016

Reference yield:

: 696-62-8
para-iodoanisole

: 110936-12-4
N-(methylcarbamoyl)homotyrosine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 49 percent / aq. NaHCO₃, Pd(OAc)2, Bu₄NCl / 24 h / 45 °C

2: H₂ / 10 percent Pd/C / methanol / 4 h / Ambient temperature

3: aq. NaHCO₃ / dioxane / 5 h / Ambient temperature

With palladium diacetate; tetrabutyl-ammonium chloride; hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In 1,4-dioxane; methanol;
DOI:10.1248/cpb.46.1094

Reference yield:

: 171077-29-5
-2-<(benzyloxycarbonyl)amino>-4-(4-methoxyphenyl)-3-butenoic acid

: 110936-12-4
N-(methylcarbamoyl)homotyrosine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10 percent Pd/C / methanol / 4 h / Ambient temperature

2: aq. NaHCO₃ / dioxane / 5 h / Ambient temperature

With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In 1,4-dioxane; methanol;
DOI:10.1248/cpb.46.1094