de-6-MSA-pactamycate

Base Information

Chemical Name:de-6-MSA-pactamycate
CAS No.:1073233-88-1
Molecular Formula:C₁₈H₂₅N₃O₆
Molecular Weight:379.413
Hs Code.:

Synonyms:de-6-MSA-pactamycate

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Chemical Property of de-6-MSA-pactamycate

Chemical Property:

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Technology Process of de-6-MSA-pactamycate

There total 33 articles about de-6-MSA-pactamycate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1295471-72-5
C₁₈H₂₃N₅O₆

: 1073233-88-1
de-6-MSA-pactamycate

Guidance literature:: With ammonium chloride; zinc; In tetrahydrofuran; ethanol; water; at 20 ℃; for 6h;
DOI:10.1021/jo301638z

Reference yield:

: C₃₉H₅₀F₃NO₈SSi₂

: 1073233-88-1
de-6-MSA-pactamycate

Guidance literature:: Multi-step reaction with 16 steps

1: tetrabutylammoniun azide / toluene / 20 °C

2: trifluoroacetic acid / acetonitrile; water / 0 - 20 °C

3: Dess-Martin periodane / dichloromethane / 0 - 20 °C

4: tetrahydrofuran / -78 °C

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

6: zinc trifluoromethanesulfonate; acetic acid / 80 °C

7: potassium carbonate / methanol / 20 °C

8: triethylamine; dmap / 0 - 20 °C

9: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / -78 - 0 °C

10: ytterbium(III) triflate / toluene / 80 °C

11: sodium cyanoborohydride; acetic acid / toluene / 12 h / 40 °C / Inert atmosphere

12: pyrographite; triethylamine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

13: 4-methylmorpholine N-oxide; osmium(VIII) oxide; water / acetone; tetrahydrofuran / 2 h / 20 °C

14: sodium periodate / water; tetrahydrofuran / 3 h / 20 °C

15: trifluoroacetic acid / neat (no solvent) / 40 °C

16: ammonium chloride; zinc / water; tetrahydrofuran; ethanol / 6 h / 20 °C

With pyridine; dmap; sodium periodate; osmium(VIII) oxide; trifluoromethylsulfonic anhydride; tetrabutyl ammonium fluoride; water; tetrabutylammoniun azide; zinc trifluoromethanesulfonate; sodium cyanoborohydride; potassium carbonate; pyrographite; ammonium chloride; Dess-Martin periodane; acetic acid; 4-methylmorpholine N-oxide; triethylamine; trifluoroacetic acid; ytterbium(III) triflate; zinc; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetone; toluene; acetonitrile;
DOI:10.1021/jo301638z

Reference yield:

: 1295471-16-7
C₃₈H₅₀N₄O₅Si₂

: 1073233-88-1
de-6-MSA-pactamycate

Guidance literature:: Multi-step reaction with 15 steps

1: trifluoroacetic acid / acetonitrile; water / 0 - 20 °C

2: Dess-Martin periodane / dichloromethane / 0 - 20 °C

3: tetrahydrofuran / -78 °C

4: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C

5: zinc trifluoromethanesulfonate; acetic acid / 80 °C

6: potassium carbonate / methanol / 20 °C

7: triethylamine; dmap / 0 - 20 °C

8: pyridine; trifluoromethylsulfonic anhydride / dichloromethane / -78 - 0 °C

9: ytterbium(III) triflate / toluene / 80 °C

10: sodium cyanoborohydride; acetic acid / toluene / 12 h / 40 °C / Inert atmosphere

11: pyrographite; triethylamine / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

12: 4-methylmorpholine N-oxide; osmium(VIII) oxide; water / acetone; tetrahydrofuran / 2 h / 20 °C

13: sodium periodate / water; tetrahydrofuran / 3 h / 20 °C

14: trifluoroacetic acid / neat (no solvent) / 40 °C

15: ammonium chloride; zinc / water; tetrahydrofuran; ethanol / 6 h / 20 °C

With pyridine; dmap; sodium periodate; osmium(VIII) oxide; trifluoromethylsulfonic anhydride; tetrabutyl ammonium fluoride; water; zinc trifluoromethanesulfonate; sodium cyanoborohydride; potassium carbonate; pyrographite; ammonium chloride; Dess-Martin periodane; acetic acid; 4-methylmorpholine N-oxide; triethylamine; trifluoroacetic acid; ytterbium(III) triflate; zinc; In tetrahydrofuran; methanol; ethanol; dichloromethane; water; acetone; toluene; acetonitrile;
DOI:10.1021/jo301638z