Technology Process of C24H28Cl2N6O4S
There total 6 articles about C24H28Cl2N6O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate;
In
water; acetonitrile;
at 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium ethanolate / ethanol / 1 h / 20 - 70 °C / Inert atmosphere
2: hydrogen / palladium 10% on activated carbon / ethanol / 1.5 h / 20 °C / Inert atmosphere
3: trichlorophosphate / 5 h / 20 - 100 °C
4: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere
5: sodium hydrogencarbonate / acetonitrile; water / 1 h / 20 °C
With
hydrogen; sodium ethanolate; sodium hydrogencarbonate; triethylamine; trichlorophosphate;
palladium 10% on activated carbon;
In
ethanol; dichloromethane; water; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
1.2: 1 h
2.1: sodium ethanolate / ethanol / 1 h / 20 - 70 °C / Inert atmosphere
3.1: hydrogen / palladium 10% on activated carbon / ethanol / 1.5 h / 20 °C / Inert atmosphere
4.1: trichlorophosphate / 5 h / 20 - 100 °C
5.1: triethylamine / dichloromethane / 1 h / 20 °C / Inert atmosphere
6.1: sodium hydrogencarbonate / acetonitrile; water / 1 h / 20 °C
With
n-butyllithium; hydrogen; sodium ethanolate; sodium hydrogencarbonate; triethylamine; trichlorophosphate;
palladium 10% on activated carbon;
In
tetrahydrofuran; ethanol; dichloromethane; water; acetonitrile;