phenyl 4,6-O-p-methoxybenzylidene-2-O-(2-methylnaphthyl)-3-O-(triisopropylsilyloxymethyl)-1-thio-α-D-mannopyranoside

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Chemical Name:phenyl 4,6-O-p-methoxybenzylidene-2-O-(2-methylnaphthyl)-3-O-(triisopropylsilyloxymethyl)-1-thio-α-D-mannopyranoside
CAS No.:1250346-22-5
Molecular Formula:C₄₁H₅₂O₇SSi
Molecular Weight:717.011
Hs Code.:

Synonyms:phenyl 4,6-O-p-methoxybenzylidene-2-O-(2-methylnaphthyl)-3-O-(triisopropylsilyloxymethyl)-1-thio-α-D-mannopyranoside

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Chemical Property of phenyl 4,6-O-p-methoxybenzylidene-2-O-(2-methylnaphthyl)-3-O-(triisopropylsilyloxymethyl)-1-thio-α-D-mannopyranoside

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Technology Process of phenyl 4,6-O-p-methoxybenzylidene-2-O-(2-methylnaphthyl)-3-O-(triisopropylsilyloxymethyl)-1-thio-α-D-mannopyranoside

There total 1 articles about phenyl 4,6-O-p-methoxybenzylidene-2-O-(2-methylnaphthyl)-3-O-(triisopropylsilyloxymethyl)-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1250346-13-4
phenyl 4,6-O-p-methoxybenzylidene-3-O-(triisopropylsilyloxymethyl)-1-thio-α-D-mannopyranoside

: 939-26-4
2-bromomethylnaphthyl bromide

: 1250346-22-5
phenyl 4,6-O-p-methoxybenzylidene-2-O-(2-methylnaphthyl)-3-O-(triisopropylsilyloxymethyl)-1-thio-α-D-mannopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; for 1h;
DOI:10.1021/ol101951u

Reference yield: 63.0%

: 1250346-40-7
allyl 3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

: 1250346-22-5
phenyl 4,6-O-p-methoxybenzylidene-2-O-(2-methylnaphthyl)-3-O-(triisopropylsilyloxymethyl)-1-thio-α-D-mannopyranoside

: 1250346-55-4
allyl 4,6-di-O-p-methoxybenzylidene-3-O-(triisopropylsilyloxymethyl)-2-O-(2-methylnaphthyl)-β-D-mannopyranosyl-(1-4)-3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside

Guidance literature:: phenyl 4,6-O-p-methoxybenzylidene-2-O-(2-methylnaphthyl)-3-O-(triisopropylsilyloxymethyl)-1-thio-α-D-mannopyranoside; With 4-nitrobenzenesulfenyl chloride; 2,6-di-tert-butyl-4-methylpyridine; silver trifluoromethanesulfonate; In dichloromethane; at -78 - 20 ℃; for 0.416667h; Molecular sieve; Darkness;

allyl 3,6-di-O-benzyl-2-O-levulinoyl-α-D-mannopyranoside; In dichloromethane; at -78 ℃; for 1h; Molecular sieve;
DOI:10.1021/ol101951u