<β-<3,4-(methylenedioxy)phenyl>cyclohex-2-enyl>acetohydroxamic acid

Base Information

Chemical Name:<β-<3,4-(methylenedioxy)phenyl>cyclohex-2-enyl>acetohydroxamic acid
CAS No.:82201-79-4
Molecular Formula:C₁₅H₁₇NO₄
Molecular Weight:275.304
Hs Code.:

Synonyms:<β-<3,4-(methylenedioxy)phenyl>cyclohex-2-enyl>acetohydroxamic acid

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Chemical Property of <β-<3,4-(methylenedioxy)phenyl>cyclohex-2-enyl>acetohydroxamic acid

Chemical Property:

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Technology Process of <β-<3,4-(methylenedioxy)phenyl>cyclohex-2-enyl>acetohydroxamic acid

There total 7 articles about <β-<3,4-(methylenedioxy)phenyl>cyclohex-2-enyl>acetohydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (1-Benzo[1,3]dioxol-5-yl-cyclohex-2-enyl)-acetyl chloride

: 82201-79-4
<β-<3,4-(methylenedioxy)phenyl>cyclohex-2-enyl>acetohydroxamic acid

Guidance literature:: With hydroxylamine hydrochloride; sodium carbonate; In diethyl ether; water; benzene; for 12h; Yield given; Ambient temperature;
DOI:10.1016/S0040-4020(01)93275-2

Reference yield:

: 82201-78-3
<β-<3,4-(methylenedioxy)phenyl>cyclohex-2-enyl>acetic acid

: 82201-79-4
<β-<3,4-(methylenedioxy)phenyl>cyclohex-2-enyl>acetohydroxamic acid

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / benzene / 2 h / Heating

2: NH₂OH*HCl, Na₂CO₃ / benzene; diethyl ether / 0.08 h

With thionyl chloride; hydroxylamine hydrochloride; sodium carbonate; In diethyl ether; benzene;
DOI:10.1021/ja00401a039

Reference yield:

: 274-09-9
Methylenedioxybenzene

: 82201-79-4
<β-<3,4-(methylenedioxy)phenyl>cyclohex-2-enyl>acetohydroxamic acid

Guidance literature:: Multi-step reaction with 7 steps

1: 85 percent / Br₂ / acetic acid / 1 h

2: 1.) n-BuLi / 1.) Et₂O, 0 deg C

3: NaBH₄ / ethanol / -22 °C

4: pyridine / 10 h

5: 1.) LDA, HMPA, 2.) t-BuMe₂SiCl, 3.) AcOH

6: SOCl₂ / benzene / 2 h / Heating

7: NH₂OH*HCl, Na₂CO₃ / benzene; diethyl ether / 0.08 h

With pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; n-butyllithium; thionyl chloride; hydroxylamine hydrochloride; bromine; sodium carbonate; tert-butyldimethylsilyl chloride; acetic acid; lithium diisopropyl amide; In diethyl ether; ethanol; acetic acid; benzene;
DOI:10.1021/ja00401a039