1,1-bis(ethylsulfanyl)-4-phenyl-2-trifluoromethylbut-1-en-3-yne

Base Information

• Chemical Name: 1,1-bis(ethylsulfanyl)-4-phenyl-2-trifluoromethylbut-1-en-3-yne
• CAS No.: 1057658-07-7
• Molecular Formula: C₁₅H₁₅F₃S₂
• Molecular Weight: 316.411
• Mol file: 1057658-07-7.mol

Synonyms:1,1-bis(ethylsulfanyl)-4-phenyl-2-trifluoromethylbut-1-en-3-yne

Chemical Property of 1,1-bis(ethylsulfanyl)-4-phenyl-2-trifluoromethylbut-1-en-3-yne

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,1-bis(ethylsulfanyl)-4-phenyl-2-trifluoromethylbut-1-en-3-yne

There total 1 articles about 1,1-bis(ethylsulfanyl)-4-phenyl-2-trifluoromethylbut-1-en-3-yne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

Bis(ethylthio)(1,2,2,2-tetrafluoroethylidene)methane (145327-75-9) + 1-Phenyl-2-(trimethylsilyl)acetylene (2170-06-1) → 1,1-bis(ethylsulfanyl)-4-phenyl-2-trifluoromethylbut-1-en-3-yne (1057658-07-7)

Guidance literature:

With tetramethylammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1016/j.jfluchem.2007.07.014

Reference yield: 100.0%

1,1-bis(ethylsulfanyl)-4-phenyl-2-trifluoromethylbut-1-en-3-yne (1057658-07-7) + Hexanethiol (111-31-9) → 1,1-bis(ethylsulfanyl)-3-hexylsulfanyl-4-phenyl-2-trifluoromethylbuta-1,3-diene

Guidance literature:

With trifluoroacetic acid; at 20 ℃; for 2h;

DOI:10.1016/j.jfluchem.2007.07.014

Reference yield: 73.0%

1,1-bis(ethylsulfanyl)-4-phenyl-2-trifluoromethylbut-1-en-3-yne (1057658-07-7) → S-ethyl 3-oxo-4-phenyl-2-trifluoromethylbutanthioate

Guidance literature:

With water; trifluoroacetic acid; at 70 - 75 ℃; for 2h;

DOI:10.1016/j.jfluchem.2007.07.014

upstream raw materials:

Bis(ethylthio)(1,2,2,2-tetrafluoroethylidene)methane

1-Phenyl-2-(trimethylsilyl)acetylene