para-chlorophenyl 6-azido-2,6-dideoxy-2-fluoro-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:para-chlorophenyl 6-azido-2,6-dideoxy-2-fluoro-1-thio-β-D-galactopyranoside
CAS No.:813432-83-6
Molecular Formula:C₁₂H₁₃ClFN₃O₃S
Molecular Weight:333.771
Hs Code.:

Synonyms:para-chlorophenyl 6-azido-2,6-dideoxy-2-fluoro-1-thio-β-D-galactopyranoside

Suppliers and Price of para-chlorophenyl 6-azido-2,6-dideoxy-2-fluoro-1-thio-β-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of para-chlorophenyl 6-azido-2,6-dideoxy-2-fluoro-1-thio-β-D-galactopyranoside

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of para-chlorophenyl 6-azido-2,6-dideoxy-2-fluoro-1-thio-β-D-galactopyranoside

There total 4 articles about para-chlorophenyl 6-azido-2,6-dideoxy-2-fluoro-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: para-chlorophenyl 2-deoxy-2-fluoro-6-O-tosyl-1-thio-β-D-galactopyranoside

: 813432-83-6
para-chlorophenyl 6-azido-2,6-dideoxy-2-fluoro-1-thio-β-D-galactopyranoside

Guidance literature:: With sodium azide; In N,N-dimethyl-formamide; at 70 ℃;
DOI:10.1002/anie.200454235

Reference yield:

: 93253-40-8
3,4,6-tri-O-acetyl-2-deoxy-2-fluoro-α-D-galactopyranosyl bromide

: 813432-83-6
para-chlorophenyl 6-azido-2,6-dideoxy-2-fluoro-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: tetrabutylammonium hydrogen sulfate; NaOH / CH₂Cl₂ / 20 °C

2: 1.32 g / NaOMe / methanol / 0.83 h / 20 °C

3: pyridine / 4 h / 0 - 20 °C

4: 310 mg / sodium azide / dimethylformamide / 70 °C

With pyridine; sodium hydroxide; sodium azide; sodium methylate; tetra(n-butyl)ammonium hydrogensulfate; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/anie.200454235

Reference yield:

: 813432-82-5
para-chlorophenyl 2-deoxy-2-fluoro-1-thio-β-D-galactopyranoside

: 813432-83-6
para-chlorophenyl 6-azido-2,6-dideoxy-2-fluoro-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 4 h / 0 - 20 °C

2: 310 mg / sodium azide / dimethylformamide / 70 °C

With pyridine; sodium azide; In N,N-dimethyl-formamide;
DOI:10.1002/anie.200454235