9-(o-tert-butylphenyl)-9-hydroxyfluorenecarboxylic acid

Base Information

Chemical Name:9-(o-tert-butylphenyl)-9-hydroxyfluorenecarboxylic acid
CAS No.:675125-87-8
Molecular Formula:C₂₄H₂₂O₃
Molecular Weight:358.437
Hs Code.:

Synonyms:9-(o-tert-butylphenyl)-9-hydroxyfluorenecarboxylic acid

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Chemical Property of 9-(o-tert-butylphenyl)-9-hydroxyfluorenecarboxylic acid

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Technology Process of 9-(o-tert-butylphenyl)-9-hydroxyfluorenecarboxylic acid

There total 3 articles about 9-(o-tert-butylphenyl)-9-hydroxyfluorenecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6310-21-0
2-(1,1-dimethylethyl)-benzenamine

: 675125-87-8
9-(o-tert-butylphenyl)-9-hydroxyfluorenecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: aq. HBr; NaNO₂; Cu

2.1: Mg / tetrahydrofuran / 0.83 h / Heating

2.2: tetrahydrofuran / 10 h / Heating

With hydrogen bromide; copper; magnesium; sodium nitrite; In tetrahydrofuran;
DOI:10.1021/jo0351015

Reference yield:

: 7073-99-6
2-tert-butylbromobenzene

: potassium 9-oxo-9H-fluorene-2-carboxylate

: 675125-87-8
9-(o-tert-butylphenyl)-9-hydroxyfluorenecarboxylic acid

Guidance literature:: 2-tert-butylbromobenzene; With magnesium; In tetrahydrofuran; for 0.833333h; Heating;

potassium 9-oxo-9H-fluorene-2-carboxylate; In tetrahydrofuran; for 10h; Heating;
DOI:10.1021/jo0351015