12-(phenylsulfonyl)-12H-indolo[3,2-j]phenanthridin-7-ol

Base Information

Chemical Name:12-(phenylsulfonyl)-12H-indolo[3,2-j]phenanthridin-7-ol
CAS No.:1597408-95-1
Molecular Formula:C₂₅H₁₆N₂O₃S
Molecular Weight:424.48
Hs Code.:

Synonyms:12-(phenylsulfonyl)-12H-indolo[3,2-j]phenanthridin-7-ol

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Chemical Property of 12-(phenylsulfonyl)-12H-indolo[3,2-j]phenanthridin-7-ol

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Technology Process of 12-(phenylsulfonyl)-12H-indolo[3,2-j]phenanthridin-7-ol

There total 14 articles about 12-(phenylsulfonyl)-12H-indolo[3,2-j]phenanthridin-7-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1445973-98-7
4-hydroxy-2-(2-nitrophenyl)-9-(phenylsulfonyl)-9H-carbazole-3-carbaldehyde

: 1597408-95-1
12-(phenylsulfonyl)-12H-indolo[3,2-j]phenanthridin-7-ol

Guidance literature:: With iron; calcium chloride; In ethanol; water; for 5h; Inert atmosphere; Reflux;
DOI:10.1002/ejoc.201301524

Reference yield:

: 1445973-84-1
(E)-1-(2-(2-nitrostyryl)-1-(phenylsulfonyl)-1H-indol-3-yl)ethanone

: 1597408-95-1
12-(phenylsulfonyl)-12H-indolo[3,2-j]phenanthridin-7-ol

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetrahydrofuran / 1 h / 10 °C

2.1: N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

3.1: potassium carbonate / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere

3.2: 24 h / Reflux; Inert atmosphere

4.1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 2 h / Inert atmosphere; Reflux

5.1: tetra(n-butyl)ammonium dichromate(VI) / chloroform / 10 h / Inert atmosphere; Reflux

6.1: boron tribromide / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

7.1: iron; calcium chloride / water; ethanol / 5 h / Inert atmosphere; Reflux

With N-Bromosuccinimide; tetra(n-butyl)ammonium dichromate(VI); 2,2'-azobis(isobutyronitrile); boron tribromide; iron; potassium carbonate; calcium chloride; In tetrahydrofuran; tetrachloromethane; ethanol; dichloromethane; chloroform; water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201301524

Reference yield:

: 1597408-89-3
4-methoxy-2-(2-nitrophenyl)-9-(phenylsulfonyl)-9H-carbazole-3-carbaldehyde

: 1597408-95-1
12-(phenylsulfonyl)-12H-indolo[3,2-j]phenanthridin-7-ol

Guidance literature:: Multi-step reaction with 2 steps

1: boron tribromide / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

2: iron; calcium chloride / water; ethanol / 5 h / Inert atmosphere; Reflux

With boron tribromide; iron; calcium chloride; In ethanol; dichloromethane; water;
DOI:10.1002/ejoc.201301524