4-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methoxy)-N,N-dimethylaniline

Base Information

Chemical Name:4-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methoxy)-N,N-dimethylaniline
CAS No.:1443828-14-5
Molecular Formula:C₂₀H₂₆N₂O₃
Molecular Weight:342.438
Hs Code.:

Synonyms:4-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methoxy)-N,N-dimethylaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methoxy)-N,N-dimethylaniline

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Technology Process of 4-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methoxy)-N,N-dimethylaniline

There total 2 articles about 4-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methoxy)-N,N-dimethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1443828-00-9
C₂₀H₂₄N₂O₃

: 1443828-14-5
4-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methoxy)-N,N-dimethylaniline

Guidance literature:: With methanol; sodium tetrahydroborate; at 0 - 20 ℃; for 18h; Inert atmosphere;
DOI:10.1021/jm400177t

Reference yield:

: 1443827-85-7
N-(3,4-dimethoxyphenylethyl)-2-(4-(dimethylamino)phenoxy)acetamide

: 1443828-14-5
4-((6,7-dimethoxy-1,2,3,4-tetrahydroisoquinolin-1-yl)methoxy)-N,N-dimethylaniline

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / toluene / 1.5 h / Reflux

2: sodium tetrahydroborate; methanol / 18 h / 0 - 20 °C / Inert atmosphere

With methanol; sodium tetrahydroborate; trichlorophosphate; In toluene;
DOI:10.1021/jm400177t