Oxireno[7,8]naphtho[1,2-b]furan-7(2H)-one,decahydro-3-hydroxy-3a,6,8c-trimethyl-,[1aR-(1aR,3â,3aR,5aâ,6â,8aR,8bâ,8cR)]-

Base Information

Chemical Name:Oxireno[7,8]naphtho[1,2-b]furan-7(2H)-one,decahydro-3-hydroxy-3a,6,8c-trimethyl-,[1aR-(1aR,3â,3aR,5aâ,6â,8aR,8bâ,8cR)]-
CAS No.:66428-34-0
Molecular Formula:C₁₅H₂₂O₄
Molecular Weight:266.337
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Oxireno[7,8]naphtho[1,2-b]furan-7(2H)-one,decahydro-3-hydroxy-3a,6,8c-trimethyl-,[1aR-(1aR,3â,3aR,5aâ,6â,8aR,8bâ,8cR)]-

Chemical Property:

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Safty Information:

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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Oxireno[7,8]naphtho[1,2-b]furan-7(2H)-one,decahydro-3-hydroxy-3a,6,8c-trimethyl-,[1aR-(1aR,3â,3aR,5aâ,6â,8aR,8bâ,8cR)]-

There total 2 articles about Oxireno[7,8]naphtho[1,2-b]furan-7(2H)-one,decahydro-3-hydroxy-3a,6,8c-trimethyl-,[1aR-(1aR,3â,3aR,5aâ,6â,8aR,8bâ,8cR)]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3863-32-9,46943-34-4,66428-34-0,101540-24-3
11β,13-dihydrosantamarin 3,4α-epoxide

Guidance literature:: In dichloromethane; Ambient temperature; peracid oxidation;
DOI:10.1016/0031-9422(90)87104-3

Reference yield:

: 3863-32-9,46943-34-4,66428-34-0,101540-24-3
3,4-Epoxy-1β-hydroxy-santan-5,12-olid C

Guidance literature:: Aus 1β-Hydroxy-sant-3-en-5,12-olid C (IIa), Erw. mit 3-Chlor-perbenzoesaeure in CHCl3;
DOI:10.1016/S0040-4020(01)98644-2

Reference yield:

: 66428-34-0
(11S)-3α,4α-Epoxy-1α-hydroxyeudesmano-13,6α-lactone

: 84927-80-0
(11S)-6α,14-Dihydroxy-2,3-secoeudesma-1,3-dien-13-oic Acid

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / chromic anhydride / CH₂Cl₂; pyridine / 12 h / 0 °C

2: 49 percent / zinc borohydride / 1,2-dimethoxy-ethane / 1 h / Ambient temperature

3: 98 percent / pyridine / 16.5 h / Ambient temperature

4: 68 percent / toluene / 72 h / Heating

5: 100 percent / 1 M KOH aqueous / ethanol / 0.5 h / 50 - 55 °C

With chromium(VI) oxide; potassium hydroxide; zinc borohydride; In pyridine; 1,2-dimethoxyethane; ethanol; dichloromethane; toluene;
DOI:10.1021/jo00156a014