methyl 3-benzamido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-altropyranoside

Base Information

Chemical Name:methyl 3-benzamido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-altropyranoside
CAS No.:95341-75-6
Molecular Formula:C₂₁H₂₂FNO₅
Molecular Weight:387.408
Hs Code.:

Synonyms:methyl 3-benzamido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-altropyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-benzamido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-altropyranoside

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Technology Process of methyl 3-benzamido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-altropyranoside

There total 1 articles about methyl 3-benzamido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-altropyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 99388-52-0
benzyl 4,6-O-benzylidene-2,3-benzoylepimino-2,3-dideoxy-α-D-allopyranoside

: 99388-53-1
benzyl 2-benzamido-4,6-O-benzylidene-2,3-dideoxy-3-fluoro-α-D-glucopyranoside

: 95341-75-6
methyl 3-benzamido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-altropyranoside

: 73793-32-5
benzyl 4,6-O-benzylidene-2,3-dideoxy-2,3-epimino-α-D-allopyranoside

Guidance literature:: With tetrabutyl ammonium fluoride; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 80 ℃; for 1h;
DOI:10.1016/0008-6215(85)85048-5

Reference yield: 41.0%

: 95341-75-6
methyl 3-benzamido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-altropyranoside

: 95239-45-5
methyl 3-benzamido-4-O-benzoyl-6-bromo-2,3,6-trideoxy-2-fluoro-α-D-altropyranoside

Guidance literature:: With N-Bromosuccinimide; barium carbonate; In tetrachloromethane; for 2h; Heating;
DOI:10.1016/0008-6215(85)85048-5

Reference yield:

: 95341-75-6
methyl 3-benzamido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-α-D-altropyranoside

: 99388-62-2
methyl 3-benzamido-2,3,6-trideoxy-2-fluoro-β-L-galactopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 41 percent / N-bromosuccinimide, barium carbonate / CCl₄ / 2 h / Heating

2: 92 percent / silver fluoride / pyridine / 24 h / Ambient temperature; dark

3: 86 percent / sodium methoxide / methanol / 1 h / Ambient temperature

4: 67 percent / H₂ / 10percent Pd/C / methanol / 24 h

With N-Bromosuccinimide; hydrogen; sodium methylate; silver fluoride; barium carbonate; palladium on activated charcoal; In pyridine; methanol; tetrachloromethane;
DOI:10.1016/0008-6215(85)85048-5