[4-[2-Chloroethyl(methyl)amino]phenyl]arsonic acid

Base Information

Chemical Name:[4-[2-Chloroethyl(methyl)amino]phenyl]arsonic acid
CAS No.:5185-72-8
Molecular Formula:C₉H₁₃AsClNO₃
Molecular Weight:293.582
Hs Code.:
DSSTox Substance ID:DTXSID80199805
Nikkaji Number:J55.396D
Mol file:5185-72-8.mol

Synonyms:5185-72-8;BRN 2841702;p-ARSANILIC ACID, N-(2-CHLOROETHYL)-N-METHYL-;N-(2-Chloroethyl)-N-methyl-p-arsanilic acid;[4-[2-chloroethyl(methyl)amino]phenyl]arsonic acid;C9H13AsClNO3;C9-H13-As-Cl-N-O3;DTXSID80199805;LS-21696;Arsanilic acid, N-(2-chloroethyl)-N-methyl-

Suppliers and Price of [4-[2-Chloroethyl(methyl)amino]phenyl]arsonic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of [4-[2-Chloroethyl(methyl)amino]phenyl]arsonic acid

Chemical Property:

Vapor Pressure:2.02E-11mmHg at 25°C
Boiling Point:514.8°Cat760mmHg
Flash Point:265.1°C
PSA：60.77000
Density:g/cm³
LogP:-0.07740
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:4
Exact Mass:292.979991
Heavy Atom Count:15
Complexity:238

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN(CCCl)C1=CC=C(C=C1)[As](=O)(O)O

Technology Process of [4-[2-Chloroethyl(methyl)amino]phenyl]arsonic acid

There total 3 articles about [4-[2-Chloroethyl(methyl)amino]phenyl]arsonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1669-85-8
N-(2-chloroethyl)-N-methylaniline

: 5185-72-8
N-Methyl-N-(2-chloroethyl)-p-arsanilic Acid

Guidance literature:: Multi-step reaction with 3 steps

1: (nitrosation)

2: SnCl₂, aq. HCl

3: (i) NaNO₂, aq. HCl, (ii) aq. Na₃AsO₃, CuSO₄*5H₂O

With hydrogenchloride; tin(ll) chloride;
DOI:10.1021/jm00320a016

Reference yield:

: 93-90-3
N-(2-hydroxyethyl)-N-methylaminobenzene

: 5185-72-8
N-Methyl-N-(2-chloroethyl)-p-arsanilic Acid

Guidance literature:: Multi-step reaction with 4 steps

1: POCl₃

2: (nitrosation)

3: SnCl₂, aq. HCl

4: (i) NaNO₂, aq. HCl, (ii) aq. Na₃AsO₃, CuSO₄*5H₂O

With hydrogenchloride; tin(ll) chloride; trichlorophosphate;
DOI:10.1021/jm00320a016

Reference yield:

: 5185-74-0
N-(2-chloro-ethyl)-N-methyl-4-nitroso-aniline

: 5185-72-8
N-Methyl-N-(2-chloroethyl)-p-arsanilic Acid

Guidance literature:: Multi-step reaction with 2 steps

1: SnCl₂, aq. HCl

2: (i) NaNO₂, aq. HCl, (ii) aq. Na₃AsO₃, CuSO₄*5H₂O

With hydrogenchloride; tin(ll) chloride;
DOI:10.1021/jm00320a016