di-tert-butyl 1-(4-methoxybenzyl)-3-methylenepyrrolidine-2,2-dicarboxylate

Base Information

Chemical Name:di-tert-butyl 1-(4-methoxybenzyl)-3-methylenepyrrolidine-2,2-dicarboxylate
CAS No.:1258537-83-5
Molecular Formula:C₂₃H₃₃NO₅
Molecular Weight:403.519
Hs Code.:

Synonyms:di-tert-butyl 1-(4-methoxybenzyl)-3-methylenepyrrolidine-2,2-dicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di-tert-butyl 1-(4-methoxybenzyl)-3-methylenepyrrolidine-2,2-dicarboxylate

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Technology Process of di-tert-butyl 1-(4-methoxybenzyl)-3-methylenepyrrolidine-2,2-dicarboxylate

There total 2 articles about di-tert-butyl 1-(4-methoxybenzyl)-3-methylenepyrrolidine-2,2-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1258537-71-1
di-tert-butyl 2-(but-3-yn-1-yl(4-methoxybenzyl)amino)malonate

: 1258537-83-5
di-tert-butyl 1-(4-methoxybenzyl)-3-methylenepyrrolidine-2,2-dicarboxylate

Guidance literature:: With zinc(II) iodide; In 1,2-dichloro-ethane; at 100 ℃; for 15h; Sealed tube;
DOI:10.1002/adsc.201100401

Reference yield: 58.0%

: 591-50-4
iodobenzene

: 1258537-71-1
di-tert-butyl 2-(but-3-yn-1-yl(4-methoxybenzyl)amino)malonate

: 1258537-83-5
di-tert-butyl 1-(4-methoxybenzyl)-3-methylenepyrrolidine-2,2-dicarboxylate

: 1258537-78-8
(E)-di-tert-butyl 3-benzylidene-1-(4-methoxybenzyl)pyrrolidine-2,2-dicarboxylate

Guidance literature:: di-tert-butyl 2-(but-3-yn-1-yl(4-methoxybenzyl)amino)malonate; With sodium hexamethyldisilazane; In tetrahydrofuran; toluene; at 20 ℃;

iodobenzene; With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; copper(l) iodide; In tetrahydrofuran; toluene; at 20 ℃; for 0.166667h;
DOI:10.1002/chem.201001951