m-Chlorphenyliod(III)-difluorid

Base Information

• Chemical Name: m-Chlorphenyliod(III)-difluorid
• CAS No.: 58636-77-4
• Molecular Formula: C₆H₄ClF₂I
• Molecular Weight: 276.452

Synonyms:m-Chlorphenyliod(III)-difluorid

Chemical Property of m-Chlorphenyliod(III)-difluorid

Chemical Property:

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Technology Process of m-Chlorphenyliod(III)-difluorid

There total 2 articles about m-Chlorphenyliod(III)-difluorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-iodochlorobenzene (625-99-0) → m-Chlorphenyliod(III)-difluorid (58636-77-4)

Guidance literature:

With fluorine; In trichlorofluoromethane; at -78 ℃;

DOI:10.1016/S0022-1139(00)82593-2

Reference yield:

→ m-Chlorphenyliod(III)-difluorid (58636-77-4)

Guidance literature:

m-Chloriodbenzol, CH2Cl2, HF, XeF2;

DOI:10.1016/S0022-1139(00)82108-9

Reference yield:

benzyltrimethylsilane (770-09-2) + m-Chlorphenyliod(III)-difluorid (58636-77-4) → 1-benzyl-2-chloro-4-iodobenzene

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In acetonitrile; at 20 ℃; for 1h; regioselective reaction; Inert atmosphere;

DOI:10.1002/ejoc.202000393

upstream raw materials:

3-iodochlorobenzene

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