(S)-tert-butyl 3-(2-(2-cyanoethylamino)ethyl)-3-(3,4-dichlorophenyl)piperidine-1-carboxylate

Base Information

Chemical Name:(S)-tert-butyl 3-(2-(2-cyanoethylamino)ethyl)-3-(3,4-dichlorophenyl)piperidine-1-carboxylate
CAS No.:1231958-18-1
Molecular Formula:C₂₁H₂₉Cl₂N₃O₂
Molecular Weight:426.386
Hs Code.:

Synonyms:(S)-tert-butyl 3-(2-(2-cyanoethylamino)ethyl)-3-(3,4-dichlorophenyl)piperidine-1-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-tert-butyl 3-(2-(2-cyanoethylamino)ethyl)-3-(3,4-dichlorophenyl)piperidine-1-carboxylate

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Technology Process of (S)-tert-butyl 3-(2-(2-cyanoethylamino)ethyl)-3-(3,4-dichlorophenyl)piperidine-1-carboxylate

There total 1 articles about (S)-tert-butyl 3-(2-(2-cyanoethylamino)ethyl)-3-(3,4-dichlorophenyl)piperidine-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.7%

: 1312884-08-4
(S)-tert-butyl 3-(3,4-dichlorophenyl)-3-(2-oxoethyl)piperidine-1-carboxylate

: 352-96-5,1119-28-4
3-aminopropionitrile fumarate salt

: 1231958-18-1
(S)-tert-butyl 3-(2-(2-cyanoethylamino)ethyl)-3-(3,4-dichlorophenyl)piperidine-1-carboxylate

Guidance literature:: 3-aminopropionitrile fumarate salt; With sodium acetate; In acetonitrile; at 18 - 25 ℃; for 0.5h; Inert atmosphere;

(S)-tert-butyl 3-(3,4-dichlorophenyl)-3-(2-oxoethyl)piperidine-1-carboxylate; In 1,2-dichloro-ethane; acetonitrile; at 18 - 25 ℃; for 0.5h;

With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; acetonitrile; at 25 ℃; for 18h;

Reference yield: 80.0%

: 1231958-18-1
(S)-tert-butyl 3-(2-(2-cyanoethylamino)ethyl)-3-(3,4-dichlorophenyl)piperidine-1-carboxylate

: 1231956-49-2
(S)-3-(2-(3-(3,4-dichlorophenyl)piperidin-3-yl)ethylamino)propanenitrile

Guidance literature:: (S)-tert-butyl 3-(2-(2-cyanoethylamino)ethyl)-3-(3,4-dichlorophenyl)piperidine-1-carboxylate; With trifluoroacetic acid; In dichloromethane; at 25 ℃; for 2h; Inert atmosphere;

With sodium hydroxide; In dichloromethane; at 18 - 25 ℃;