{2-Amino-6-[3-(cyclohexyl-methyl-carbamoyl)-propoxy]-4H-quinazolin-3-yl}-acetic acid 1-phenyl-ethyl ester; hydrobromide

Base Information

Chemical Name:{2-Amino-6-[3-(cyclohexyl-methyl-carbamoyl)-propoxy]-4H-quinazolin-3-yl}-acetic acid 1-phenyl-ethyl ester; hydrobromide
CAS No.:114703-85-4
Molecular Formula:BrH*C₂₉H₃₈N₄O₄
Molecular Weight:587.557
Hs Code.:

Synonyms:{2-Amino-6-[3-(cyclohexyl-methyl-carbamoyl)-propoxy]-4H-quinazolin-3-yl}-acetic acid 1-phenyl-ethyl ester; hydrobromide

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Chemical Property of {2-Amino-6-[3-(cyclohexyl-methyl-carbamoyl)-propoxy]-4H-quinazolin-3-yl}-acetic acid 1-phenyl-ethyl ester; hydrobromide

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Technology Process of {2-Amino-6-[3-(cyclohexyl-methyl-carbamoyl)-propoxy]-4H-quinazolin-3-yl}-acetic acid 1-phenyl-ethyl ester; hydrobromide

There total 4 articles about {2-Amino-6-[3-(cyclohexyl-methyl-carbamoyl)-propoxy]-4H-quinazolin-3-yl}-acetic acid 1-phenyl-ethyl ester; hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 98-85-1,13323-81-4
1-Phenylethanol

: 114703-85-4
{2-Amino-6-[3-(cyclohexyl-methyl-carbamoyl)-propoxy]-4H-quinazolin-3-yl}-acetic acid 1-phenyl-ethyl ester; hydrobromide

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / diethyl ether / 1 h / Ambient temperature

2: NaN₃ / dimethylformamide / Ambient temperature

3: 1.) hydrogen, 2.) HCl / Pd-C / ethanol / 3 h / 45 °C

With hydrogenchloride; sodium azide; hydrogen; triethylamine; palladium on activated charcoal; In diethyl ether; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00119a015

Reference yield:

: 72939-47-0
(+/-)-1-chloroacetoxy-1-phenyl-ethane

: 114703-85-4
{2-Amino-6-[3-(cyclohexyl-methyl-carbamoyl)-propoxy]-4H-quinazolin-3-yl}-acetic acid 1-phenyl-ethyl ester; hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: NaN₃ / dimethylformamide / Ambient temperature

2: 1.) hydrogen, 2.) HCl / Pd-C / ethanol / 3 h / 45 °C

With hydrogenchloride; sodium azide; hydrogen; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00119a015

Reference yield:

: Azido-acetic acid 1-phenyl-ethyl ester

: 114703-85-4
{2-Amino-6-[3-(cyclohexyl-methyl-carbamoyl)-propoxy]-4H-quinazolin-3-yl}-acetic acid 1-phenyl-ethyl ester; hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) hydrogen, 2.) HCl / Pd-C / ethanol / 3 h / 45 °C

With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00119a015