Technology Process of C30H31F4N3O5S
There total 16 articles about C30H31F4N3O5S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium fluoride; tetrakis(triphenylphosphine) palladium(0);
In
1,2-dimethoxyethane; water;
at 90 ℃;
for 2h;
Inert atmosphere;
Sealed tube;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: lithium hydroxide; water / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere; Sealed tube
2: triethylamine / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere; Sealed tube
3: ammonium acetate / toluene / 5 h / 110 °C / Inert atmosphere; Sealed tube
4: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate / 1,2-dimethoxyethane / 2 h / 90 °C / Inert atmosphere; Sealed tube
5: potassium fluoride; tetrakis(triphenylphosphine) palladium(0) / water; 1,2-dimethoxyethane / 2 h / 90 °C / Inert atmosphere; Sealed tube
With
potassium fluoride; tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; ammonium acetate; water; potassium acetate; triethylamine; lithium hydroxide;
In
tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-iodo-succinimide / tetrahydrofuran; acetonitrile / 0.17 h / Inert atmosphere; Sealed tube
1.2: 5 h / 20 °C / Inert atmosphere; Sealed tube
2.1: boron tribromide / dichloromethane / 4.16 h / -78 - 20 °C / Inert atmosphere; Sealed tube
3.1: pyridine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere; Sealed tube
3.2: 1 h / 0 - 20 °C / Inert atmosphere; Sealed tube
4.1: potassium fluoride; tetrakis(triphenylphosphine) palladium(0) / water; 1,2-dimethoxyethane / 2 h / 90 °C / Inert atmosphere; Sealed tube
With
pyridine; potassium fluoride; N-iodo-succinimide; tetrakis(triphenylphosphine) palladium(0); boron tribromide;
In
tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; acetonitrile;