Methyl 2-<(1S,4R,5R)-5-isopropenyl-4-methyl-4-vinyl-2-oxocyclohexyl>acetate

Base Information

Chemical Name:Methyl 2-<(1S,4R,5R)-5-isopropenyl-4-methyl-4-vinyl-2-oxocyclohexyl>acetate
CAS No.:229010-40-6
Molecular Formula:C₁₅H₂₂O₃
Molecular Weight:250.338
Hs Code.:

Synonyms:Methyl 2-<(1S,4R,5R)-5-isopropenyl-4-methyl-4-vinyl-2-oxocyclohexyl>acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Methyl 2-<(1S,4R,5R)-5-isopropenyl-4-methyl-4-vinyl-2-oxocyclohexyl>acetate

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Technology Process of Methyl 2-<(1S,4R,5R)-5-isopropenyl-4-methyl-4-vinyl-2-oxocyclohexyl>acetate

There total 6 articles about Methyl 2-<(1S,4R,5R)-5-isopropenyl-4-methyl-4-vinyl-2-oxocyclohexyl>acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 149404-74-0
(4R,5R)-1-Acetoxy-4-isopropenyl-5-methyl-5-vinylcyclohex-1-ene

: 229010-40-6
Methyl 2-<(1S,4R,5R)-5-isopropenyl-4-methyl-4-vinyl-2-oxocyclohexyl>acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / K₂CO₃ / methanol

2: LDA, HMPA / tetrahydrofuran; hexane / 1.) -78 deg C, 30 min, 2.) -78 to -40 deg C, 4 h

With N,N,N,N,N,N-hexamethylphosphoric triamide; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; methanol; hexane;
DOI:10.1039/a809983i

Reference yield:

: 202194-28-3
(1R,4R,5R)-5-Isopropenyl-4-methyl-2-oxo-4-vinyl-cyclohexanecarboxylic acid ethyl ester

: 229010-40-6
Methyl 2-<(1S,4R,5R)-5-isopropenyl-4-methyl-4-vinyl-2-oxocyclohexyl>acetate

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / NaH, HMPA / tetrahydrofuran / 1.) 0 deg C, 30 min, 2.) 0 deg c to r.t., 4 h

2: NaOH, H₂O / dimethylsulfoxide / 12 h / 50 °C

3: diethyl ether / 0 °C

With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium hydroxide; water; sodium hydride; In tetrahydrofuran; diethyl ether; dimethyl sulfoxide;
DOI:10.1039/a809983i

Reference yield:

: 229010-41-7
(1S,4R,5R)-5-Isopropenyl-1-methoxycarbonylmethyl-4-methyl-2-oxo-4-vinyl-cyclohexanecarboxylic acid ethyl ester

: 229010-40-6
Methyl 2-<(1S,4R,5R)-5-isopropenyl-4-methyl-4-vinyl-2-oxocyclohexyl>acetate

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH, H₂O / dimethylsulfoxide / 12 h / 50 °C

2: diethyl ether / 0 °C

With sodium hydroxide; water; In diethyl ether; dimethyl sulfoxide;
DOI:10.1039/a809983i