C₂₉H₃₄N₄O₄

Base Information

Chemical Name:C₂₉H₃₄N₄O₄
CAS No.:1396621-49-0
Molecular Formula:C₂₉H₃₄N₄O₄
Molecular Weight:502.613
Hs Code.:

C<sub>29</sub>H<sub>34</sub>N<sub>4</sub>O<sub>4</sub>

Synonyms:C₂₉H₃₄N₄O₄

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Chemical Property of C₂₉H₃₄N₄O₄

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Technology Process of C₂₉H₃₄N₄O₄

There total 12 articles about C₂₉H₃₄N₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.4%

: 1396621-36-5
2-(4-{[(3-methoxy-1-methyl-4-oxo-4,5-dihydro-1H-pyrrolo[3,2-c]quinolin-2-yl)carbonyl]-amino}piperidin-1-yl)ethyl acetate

: 103-63-9
1-phenyl-2-bromoethane

: 1396621-49-0
C₂₉H₃₄N₄O₄

Guidance literature:: 2-(4-{[(3-methoxy-1-methyl-4-oxo-4,5-dihydro-1H-pyrrolo[3,2-c]quinolin-2-yl)carbonyl]-amino}piperidin-1-yl)ethyl acetate; With sodium t-butanolate; In 1,2-dimethoxyethane; N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

With lithium bromide; at 20 ℃; for 0.166667h;

1-phenyl-2-bromoethane;
DOI:10.1016/j.bmc.2012.07.039

Reference yield:

: 6315-94-2
ethyl 2,4-dichloroquinoline-3-carboxylate

: 1396621-49-0
C₂₉H₃₄N₄O₄

Guidance literature:: Multi-step reaction with 12 steps

1.1: sodium acetate / acetic acid / 20?h / 120?°C

2.1: mineral oil; N,N-dimethyl-formamide / 15?min / Cooling with ice

2.2: 1 h / Cooling with ice

3.1: triethylamine / ethanol / 18 h / 85 °C

4.1: sodium ethanolate / 1 h / 60 °C

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.17 h / 20 °C

5.2: 4 h / 20 °C

6.1: sodium hydroxide / tetrahydrofuran; ethanol / 18 h / 20 °C

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 18 h / 20 °C

8.1: hydrogenchloride / ethyl acetate / 4 h / 20 °C

9.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 80 °C

10.1: methoxybenzene; trifluorormethanesulfonic acid; trifluoroacetic acid / 1 h / 80 °C

11.1: triethylamine / tetrahydrofuran / 4 h / 0 °C

12.1: sodium t-butanolate / N,N-dimethyl-formamide; 1,2-dimethoxyethane / 0.5 h / 0 °C

12.2: 0.17 h / 20 °C

With hydrogenchloride; trifluorormethanesulfonic acid; sodium ethanolate; sodium acetate; potassium carbonate; benzotriazol-1-ol; methoxybenzene; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; sodium hydroxide; sodium t-butanolate; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; acetic acid; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.bmc.2012.07.039

Reference yield:

: 99429-64-8
ethyl ester of 4-chloro-2-oxo-1,2-dihydroquinoline-3-carboxylic acid

: 1396621-49-0
C₂₉H₃₄N₄O₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: mineral oil; N,N-dimethyl-formamide / 15?min / Cooling with ice

1.2: 1 h / Cooling with ice

2.1: triethylamine / ethanol / 18 h / 85 °C

3.1: sodium ethanolate / 1 h / 60 °C

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.17 h / 20 °C

4.2: 4 h / 20 °C

5.1: sodium hydroxide / tetrahydrofuran; ethanol / 18 h / 20 °C

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 18 h / 20 °C

7.1: hydrogenchloride / ethyl acetate / 4 h / 20 °C

8.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 80 °C

9.1: methoxybenzene; trifluorormethanesulfonic acid; trifluoroacetic acid / 1 h / 80 °C

10.1: triethylamine / tetrahydrofuran / 4 h / 0 °C

11.1: sodium t-butanolate / N,N-dimethyl-formamide; 1,2-dimethoxyethane / 0.5 h / 0 °C

11.2: 0.17 h / 20 °C

With hydrogenchloride; trifluorormethanesulfonic acid; sodium ethanolate; potassium carbonate; benzotriazol-1-ol; methoxybenzene; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; sodium hydroxide; sodium t-butanolate; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; ethyl acetate; N,N-dimethyl-formamide; mineral oil;
DOI:10.1016/j.bmc.2012.07.039