p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthaloylamino-β-D-glucopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthaloylamino-β-D-glucopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside
CAS No.:1357000-49-7
Molecular Formula:C₅₄H₆₁NO₁₅S
Molecular Weight:996.142
Hs Code.:

Synonyms:p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthaloylamino-β-D-glucopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthaloylamino-β-D-glucopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

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Technology Process of p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthaloylamino-β-D-glucopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

There total 1 articles about p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthaloylamino-β-D-glucopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1242660-03-2
3,4,6-tri-O-acetyl-2-N-phthaloyl-β(1-2)-D-glucosaminyl-3-O-benzyl-(4,6)-benzylidene-β-D-mannopyranosyl p-octyloxyphenyl sulfoxide

: 1357000-49-7
p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthaloylamino-β-D-glucopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Guidance literature:: With triphenylphosphine; In tetrachloromethane; acetonitrile; for 2h; Reflux;
DOI:10.3987/COM-11-12332

Reference yield:

: 1357000-49-7
p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthaloylamino-β-D-glucopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

: 865488-96-6
2-(p-iodophenyl)ethyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3,4,6-tri-O-acetyl-α-D-mannopyranosyl-(1->6)-2,3,4-tri-O-acetyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: hydrazine hydrate / ethanol; water; toluene / 5 h / Reflux

2: pyridine / 5 h

3: acetic acid / tetrahydrofuran; water / 5 h / 55 °C

4: chloro-trimethyl-silane; lithium iodide / chloroform / 6 h / 0 - 20 °C

5: pyridine; dmap / 2 h / 0 - 20 °C

6: N-iodo-succinimide; trifluorormethanesulfonic acid / dichloromethane / 2.5 h / -50 °C / Molecular sieve

With pyridine; dmap; N-iodo-succinimide; chloro-trimethyl-silane; trifluorormethanesulfonic acid; hydrazine hydrate; acetic acid; lithium iodide; In tetrahydrofuran; ethanol; dichloromethane; chloroform; water; toluene;
DOI:10.3987/COM-11-12332

Reference yield:

: 1357000-49-7
p-octyloxyphenyl 3,4,6-tri-O-acetyl-2-deoxy-2-phthaloylamino-β-D-glucopyranosyl-(1->2)-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

: 1357000-51-1
p-octyloxyphenyl 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->2)-3-O-benzyl-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / ethanol; water; toluene / 5 h / Reflux

2: pyridine / 5 h

3: acetic acid / tetrahydrofuran; water / 5 h / 55 °C

With pyridine; hydrazine hydrate; acetic acid; In tetrahydrofuran; ethanol; water; toluene;
DOI:10.3987/COM-11-12332