1-(3,5-dimethylbenzyl)-3-(2,3,5,6-tetramethylbenzyl)benzimidazolium chloride

Base Information

Chemical Name:1-(3,5-dimethylbenzyl)-3-(2,3,5,6-tetramethylbenzyl)benzimidazolium chloride
CAS No.:1239882-38-2
Molecular Formula:C₂₇H₃₁N₂*Cl
Molecular Weight:419.01
Hs Code.:

Synonyms:1-(3,5-dimethylbenzyl)-3-(2,3,5,6-tetramethylbenzyl)benzimidazolium chloride

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Chemical Property of 1-(3,5-dimethylbenzyl)-3-(2,3,5,6-tetramethylbenzyl)benzimidazolium chloride

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Technology Process of 1-(3,5-dimethylbenzyl)-3-(2,3,5,6-tetramethylbenzyl)benzimidazolium chloride

There total 2 articles about 1-(3,5-dimethylbenzyl)-3-(2,3,5,6-tetramethylbenzyl)benzimidazolium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 7435-83-8
3-(chloromethyl)-1,2,4,5-tetramethylbenzene

: 1239882-56-4
1-(3,5-dimethylbenzyl)-1H-benzo[d]imidazole

: 1239882-38-2
1-(3,5-dimethylbenzyl)-3-(2,3,5,6-tetramethylbenzyl)benzimidazolium chloride

Guidance literature:: In N,N-dimethyl-formamide; at 20 ℃; for 5h; Inert atmosphere;
DOI:10.1002/ejic.201000181

Reference yield:

: 51-17-2,79351-71-6
benzoimidazole

: 1239882-38-2
1-(3,5-dimethylbenzyl)-3-(2,3,5,6-tetramethylbenzyl)benzimidazolium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / ethanol

2: N,N-dimethyl-formamide / 5 h / 20 °C / Inert atmosphere

With potassium hydroxide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1002/ejic.201000181

Reference yield: 88.0%

: 52462-29-0
[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

: 1239882-38-2
1-(3,5-dimethylbenzyl)-3-(2,3,5,6-tetramethylbenzyl)benzimidazolium chloride

: dichloro-[1-(2,3,5,6-tetramethylbenzyl)-3-(3,5-dimethylbenzyl)benzimidazol-2-ylidene]ruthenium(II)

Guidance literature:: With Cs₂CO₃; In toluene; (Ar), suspn. of benzimidazolium salt, Cs2CO3 and Ru complex (2.6:2.56:1)refluxed in degassed toluene for 5 h; filtered hot, concd., pptd.(n-hexane), crystd.(CH2Cl2/hexane), elem. anal.;
DOI:10.1002/ejic.201000181