(2R)-1-O-triethylsilyloxy-2-tert-butyldimethylsilyloxy-10-benzyloxy-decane

Base Information

Chemical Name:(2R)-1-O-triethylsilyloxy-2-tert-butyldimethylsilyloxy-10-benzyloxy-decane
CAS No.:910057-90-8
Molecular Formula:C₂₉H₅₆O₃Si₂
Molecular Weight:508.933
Hs Code.:

Synonyms:(2R)-1-O-triethylsilyloxy-2-tert-butyldimethylsilyloxy-10-benzyloxy-decane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R)-1-O-triethylsilyloxy-2-tert-butyldimethylsilyloxy-10-benzyloxy-decane

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Technology Process of (2R)-1-O-triethylsilyloxy-2-tert-butyldimethylsilyloxy-10-benzyloxy-decane

There total 3 articles about (2R)-1-O-triethylsilyloxy-2-tert-butyldimethylsilyloxy-10-benzyloxy-decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 910058-02-5
(R)-10-Benzyloxy-1-triethylsilanyloxy-decan-2-ol

: 69739-34-0
t-butyldimethylsiyl triflate

: 910057-90-8
(2R)-1-O-triethylsilyloxy-2-tert-butyldimethylsilyloxy-10-benzyloxy-decane

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at -50 ℃; for 2.5h;
DOI:10.1021/ol0614471

Reference yield:

: C₁₄H₂₁BrMgO

: 910057-90-8
(2R)-1-O-triethylsilyloxy-2-tert-butyldimethylsilyloxy-10-benzyloxy-decane

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / CuI / tetrahydrofuran / -30 - 0 °C

2: 84 percent / 2,6-lutidine / CH₂Cl₂ / 2.5 h / -50 °C

With 2,6-dimethylpyridine; copper(l) iodide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol0614471

Reference yield:

: 245326-10-7
(R)-(triethylsilyl)glycidyl ether

: 910057-90-8
(2R)-1-O-triethylsilyloxy-2-tert-butyldimethylsilyloxy-10-benzyloxy-decane

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / CuI / tetrahydrofuran / -30 - 0 °C

2: 84 percent / 2,6-lutidine / CH₂Cl₂ / 2.5 h / -50 °C

With 2,6-dimethylpyridine; copper(l) iodide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol0614471