Technology Process of 3,4,5-trimethoxy-α,α-dimethylphenethylamine hydrochloride
There total 7 articles about 3,4,5-trimethoxy-α,α-dimethylphenethylamine hydrochloride which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 69.7 percent / triethylamine / 60 h / Ambient temperature
2: 1.) zinc, ferric chloride; 2.) 12 N silfuric acid; 4.) hydrogen chloride / 1.) 95 percent ethanol, 2.) water, 40 deg C, 4 h; 3.) 30 deg C, 18 h; 4.) ether
3: 68.8 percent / thionyl chloride / 2 h / Ambient temperature
4: 96 percent / hydrogen / 10 percent palladium on charcoal / methanol
With
hydrogenchloride; thionyl chloride; sulfuric acid; hydrogen; iron(III) chloride; triethylamine; zinc;
palladium on activated charcoal;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 1.) zinc, ferric chloride; 2.) 12 N silfuric acid; 4.) hydrogen chloride / 1.) 95 percent ethanol, 2.) water, 40 deg C, 4 h; 3.) 30 deg C, 18 h; 4.) ether
2: 68.8 percent / thionyl chloride / 2 h / Ambient temperature
3: 96 percent / hydrogen / 10 percent palladium on charcoal / methanol
With
hydrogenchloride; thionyl chloride; sulfuric acid; hydrogen; iron(III) chloride; zinc;
palladium on activated charcoal;
In
methanol;
