4-({allyloxy}methyl)benzyl butyl carbonotrithioate

Base Information

• Chemical Name: 4-({allyloxy}methyl)benzyl butyl carbonotrithioate
• CAS No.: 1312424-62-6
• Molecular Formula: C₁₆H₂₂OS₃
• Molecular Weight: 326.548
• Mol file: 1312424-62-6.mol

Synonyms:4-({allyloxy}methyl)benzyl butyl carbonotrithioate

Chemical Property of 4-({allyloxy}methyl)benzyl butyl carbonotrithioate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of 4-({allyloxy}methyl)benzyl butyl carbonotrithioate

There total 2 articles about 4-({allyloxy}methyl)benzyl butyl carbonotrithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

carbon disulfide (75-15-0,12122-00-8) + 4-({allyloxy}methyl)benzyl bromide (1312424-61-5) + sodium 1-buthanethiolate (4779-86-6) → 4-({allyloxy}methyl)benzyl butyl carbonotrithioate (1312424-62-6)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 4h;

DOI:10.1021/ma200799b

Reference yield:

1,4-bis(bromomethyl)benzene (623-24-5) → 4-({allyloxy}methyl)benzyl butyl carbonotrithioate (1312424-62-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C

1.2: 2 h / 80 °C

2.1: tetrahydrofuran / 4 h / 20 °C

With sodium hydride; In tetrahydrofuran;

DOI:10.1021/ma200799b

upstream raw materials:

carbon disulfide

4-({allyloxy}methyl)benzyl bromide

sodium 1-buthanethiolate

1,4-bis(bromomethyl)benzene