N-(2-methoxyethyl)-2-<α-(benzotriazol-1-yl)pentyl>-4-phenyl-5-methylpyrrole

Base Information

Chemical Name:N-(2-methoxyethyl)-2-<α-(benzotriazol-1-yl)pentyl>-4-phenyl-5-methylpyrrole
CAS No.:175021-35-9
Molecular Formula:C₂₅H₃₀N₄O
Molecular Weight:402.539
Hs Code.:

Synonyms:N-(2-methoxyethyl)-2-<α-(benzotriazol-1-yl)pentyl>-4-phenyl-5-methylpyrrole

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Chemical Property of N-(2-methoxyethyl)-2-<α-(benzotriazol-1-yl)pentyl>-4-phenyl-5-methylpyrrole

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Technology Process of N-(2-methoxyethyl)-2-<α-(benzotriazol-1-yl)pentyl>-4-phenyl-5-methylpyrrole

There total 4 articles about N-(2-methoxyethyl)-2-<α-(benzotriazol-1-yl)pentyl>-4-phenyl-5-methylpyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 542-69-8
1-iodo-butane

: 175021-31-5
N-(2-methoxyethyl)-2-<(benzotriazol-1-yl)methyl>-4-phenyl-5-methylpyrrole

: 175021-35-9
N-(2-methoxyethyl)-2-<α-(benzotriazol-1-yl)pentyl>-4-phenyl-5-methylpyrrole

Guidance literature:: With n-butyllithium; In tetrahydrofuran; cyclohexane; 1.) -78 deg C, 1 h, 2.) -78 deg C, 1 h;
DOI:10.1021/jo951894m

Reference yield:

: 2114-00-3
2-bromo-1-phenyl-1-propanone

: 175021-35-9
N-(2-methoxyethyl)-2-<α-(benzotriazol-1-yl)pentyl>-4-phenyl-5-methylpyrrole

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / n-BuLi / tetrahydrofuran; cyclohexane / 1.) -78 deg C, 1 h, 2.) -78 deg C

2: 57 percent / propan-2-ol / Heating

3: 77 percent / n-BuLi / tetrahydrofuran; cyclohexane / 1.) -78 deg C, 1 h, 2.) -78 deg C, 1 h

With n-butyllithium; In tetrahydrofuran; cyclohexane; isopropyl alcohol;
DOI:10.1021/jo951894m

Reference yield:

: 142321-23-1
1-(1H-benzotriazol-1-yl)prop-2-yne

: 175021-35-9
N-(2-methoxyethyl)-2-<α-(benzotriazol-1-yl)pentyl>-4-phenyl-5-methylpyrrole

Guidance literature:: Multi-step reaction with 3 steps

1: 67 percent / n-BuLi / tetrahydrofuran; cyclohexane / 1.) -78 deg C, 1 h, 2.) -78 deg C

2: 57 percent / propan-2-ol / Heating

3: 77 percent / n-BuLi / tetrahydrofuran; cyclohexane / 1.) -78 deg C, 1 h, 2.) -78 deg C, 1 h

With n-butyllithium; In tetrahydrofuran; cyclohexane; isopropyl alcohol;
DOI:10.1021/jo951894m