2-O-acetyl-3,4-di-O-benzyl-β-D-fucopyranosyl fluoride

Base Information

Chemical Name:2-O-acetyl-3,4-di-O-benzyl-β-D-fucopyranosyl fluoride
CAS No.:172792-41-5
Molecular Formula:C₂₂H₂₅FO₅
Molecular Weight:388.436
Hs Code.:

Synonyms:2-O-acetyl-3,4-di-O-benzyl-β-D-fucopyranosyl fluoride

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Chemical Property of 2-O-acetyl-3,4-di-O-benzyl-β-D-fucopyranosyl fluoride

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Technology Process of 2-O-acetyl-3,4-di-O-benzyl-β-D-fucopyranosyl fluoride

There total 4 articles about 2-O-acetyl-3,4-di-O-benzyl-β-D-fucopyranosyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.4%

: 172792-40-4
2-O-acetyl-3,4-di-O-benzyl-α-D-fucopyranosyl chloride

: 172792-41-5
2-O-acetyl-3,4-di-O-benzyl-β-D-fucopyranosyl fluoride

Guidance literature:: With silver fluoride; In acetonitrile; benzene; for 16h; Ambient temperature;
DOI:10.1016/0008-6215(95)00160-U

Reference yield:

: 172792-42-6
3,4-di-O-benzyl-α-D-fucopyranose

: 172792-41-5
2-O-acetyl-3,4-di-O-benzyl-β-D-fucopyranosyl fluoride

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine

2: 94 percent / HCl(g) / diethyl ether / 2 h / Ambient temperature

3: 84.4 percent / silver fluoride / acetonitrile; benzene / 16 h / Ambient temperature

With pyridine; hydrogenchloride; silver fluoride; In diethyl ether; acetonitrile; benzene;
DOI:10.1016/0008-6215(95)00160-U

Reference yield:

: 3,4-di-O-benzyl-1,2-O-ethylidene-α-D-fucopyranose

: 172792-41-5
2-O-acetyl-3,4-di-O-benzyl-β-D-fucopyranosyl fluoride

Guidance literature:: Multi-step reaction with 4 steps

1: 77.5 percent / sulfuric acid / dioxane / 6 h / Heating

2: pyridine

3: 94 percent / HCl(g) / diethyl ether / 2 h / Ambient temperature

4: 84.4 percent / silver fluoride / acetonitrile; benzene / 16 h / Ambient temperature

With pyridine; hydrogenchloride; sulfuric acid; silver fluoride; In 1,4-dioxane; diethyl ether; acetonitrile; benzene;
DOI:10.1016/0008-6215(95)00160-U