1-(4-Methoxy-phenyl)-2-(1-methyl-2-methylsulfanyl-1,4,6,7-tetrahydro-imidazo[4,5-c]pyridin-5-yl)-ethanol

Base Information

• Chemical Name: 1-(4-Methoxy-phenyl)-2-(1-methyl-2-methylsulfanyl-1,4,6,7-tetrahydro-imidazo[4,5-c]pyridin-5-yl)-ethanol
• CAS No.: 119952-72-6
• Molecular Formula: C₁₇H₂₃N₃O₂S
• Molecular Weight: 333.455

Synonyms:1-(4-Methoxy-phenyl)-2-(1-methyl-2-methylsulfanyl-1,4,6,7-tetrahydro-imidazo[4,5-c]pyridin-5-yl)-ethanol

Chemical Property of 1-(4-Methoxy-phenyl)-2-(1-methyl-2-methylsulfanyl-1,4,6,7-tetrahydro-imidazo[4,5-c]pyridin-5-yl)-ethanol

Chemical Property:

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Technology Process of 1-(4-Methoxy-phenyl)-2-(1-methyl-2-methylsulfanyl-1,4,6,7-tetrahydro-imidazo[4,5-c]pyridin-5-yl)-ethanol

There total 3 articles about 1-(4-Methoxy-phenyl)-2-(1-methyl-2-methylsulfanyl-1,4,6,7-tetrahydro-imidazo[4,5-c]pyridin-5-yl)-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

5-[2-(4-Methoxy-phenyl)-2-oxo-ethyl]-1-methyl-2-methylsulfanyl-1H-imidazo[4,5-c]pyridin-5-ium; bromide (119952-66-8) → 1-(4-Methoxy-phenyl)-2-(1-methyl-2-methylsulfanyl-1,4,6,7-tetrahydro-imidazo[4,5-c]pyridin-5-yl)-ethanol (119952-72-6)

Guidance literature:

With sodium tetrahydroborate; In methanol; water; at 60 - 70 ℃; for 2h;

DOI:10.1007/BF00758317

Reference yield:

1-methyl-2-methylthio-1H-imidazo<4,5-c>pyridine (7321-95-1) → 1-(4-Methoxy-phenyl)-2-(1-methyl-2-methylsulfanyl-1,4,6,7-tetrahydro-imidazo[4,5-c]pyridin-5-yl)-ethanol (119952-72-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 73 percent / acetone / 4 h / Ambient temperature

2: 66 percent / NaBH₄ / methanol; H₂O / 2 h / 60 - 70 °C

With sodium tetrahydroborate; In methanol; water; acetone;

DOI:10.1007/BF00758317

Reference yield:

2-Bromo-4'-methoxyacetophenone (2632-13-5) → 1-(4-Methoxy-phenyl)-2-(1-methyl-2-methylsulfanyl-1,4,6,7-tetrahydro-imidazo[4,5-c]pyridin-5-yl)-ethanol (119952-72-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 73 percent / acetone / 4 h / Ambient temperature

2: 66 percent / NaBH₄ / methanol; H₂O / 2 h / 60 - 70 °C

With sodium tetrahydroborate; In methanol; water; acetone;

DOI:10.1007/BF00758317

upstream raw materials:

5-[2-(4-Methoxy-phenyl)-2-oxo-ethyl]-1-methyl-2-methylsulfanyl-1H-imidazo[4,5-c]pyridin-5-ium; bromide

1-methyl-2-methylthio-1H-imidazo<4,5-c>pyridine

2-Bromo-4'-methoxyacetophenone

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