(4S)-3-((E)-4'-(Benzyloxy)-2'-butenoyl)-4-(phenylmethyl)-2-oxazolidinone

Base Information

Chemical Name:(4S)-3-((E)-4'-(Benzyloxy)-2'-butenoyl)-4-(phenylmethyl)-2-oxazolidinone
CAS No.:128217-43-6
Molecular Formula:C₂₁H₂₁NO₄
Molecular Weight:351.402
Hs Code.:

Synonyms:(4S)-3-((E)-4'-(Benzyloxy)-2'-butenoyl)-4-(phenylmethyl)-2-oxazolidinone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S)-3-((E)-4'-(Benzyloxy)-2'-butenoyl)-4-(phenylmethyl)-2-oxazolidinone

Chemical Property:

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Technology Process of (4S)-3-((E)-4'-(Benzyloxy)-2'-butenoyl)-4-(phenylmethyl)-2-oxazolidinone

There total 1 articles about (4S)-3-((E)-4'-(Benzyloxy)-2'-butenoyl)-4-(phenylmethyl)-2-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 90719-32-7
(S)-4-Benzyl-2-oxazolidinone

: 162551-89-5
4-(phenylmethoxy)-2-butenoic acid

: 128217-43-6
(4S)-3-((E)-4'-(Benzyloxy)-2'-butenoyl)-4-(phenylmethyl)-2-oxazolidinone

Guidance literature:: 4-(phenylmethoxy)-2-butenoic acid; With pivaloyl chloride; triethylamine; lithium chloride; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

(S)-4-Benzyl-2-oxazolidinone; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol901372m

Reference yield: 86.0%

: 128217-43-6
(4S)-3-((E)-4'-(Benzyloxy)-2'-butenoyl)-4-(phenylmethyl)-2-oxazolidinone

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 128299-70-7
(S)-4-Benzyl-3-((1S,2R,3R,4R)-3-benzyloxymethyl-bicyclo[2.2.1]hept-5-ene-2-carbonyl)-oxazolidin-2-one

: 128385-57-9
(S)-4-Benzyl-3-((1R,2R,3R,4S)-3-benzyloxymethyl-bicyclo[2.2.1]hept-5-ene-2-carbonyl)-oxazolidin-2-one

: 128299-71-8
(S)-4-Benzyl-3-((1S,2S,3S,4R)-3-benzyloxymethyl-bicyclo[2.2.1]hept-5-ene-2-carbonyl)-oxazolidin-2-one

: 128217-44-7
(4S)-3-(((3'R,4'R,5'S,6'S)-5'-((Benzyloxy)methyl)bicyclo<2.2.1>hepten-4'-yl)carbonyl)-4-(phenylmethyl)-2-oxazolidinone

Guidance literature:: With diethylaluminium chloride; In dichloromethane; at -78 ℃; for 2h; Yields of byproduct given;
DOI:10.1021/jo00304a019

Reference yield:

: 5293-90-3
1,3,3-trimethyl-2-vinylcyclohexene

: 128217-43-6
(4S)-3-((E)-4'-(Benzyloxy)-2'-butenoyl)-4-(phenylmethyl)-2-oxazolidinone

: 1176702-25-2
C₃₂H₃₉NO₄

: C₃₂H₃₉NO₄

Guidance literature:: (4S)-3-((E)-4'-(Benzyloxy)-2'-butenoyl)-4-(phenylmethyl)-2-oxazolidinone; With methylaluminum dichloride; In dichloromethane; at -78 ℃; for 0.166667h; Inert atmosphere;

1,3,3-trimethyl-2-vinylcyclohexene; In dichloromethane; at 0 - 23 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol901372m