phenyl 2-(5-phenylpent-4-ynyl)cyclopropyl ketone

Base Information

Chemical Name:phenyl 2-(5-phenylpent-4-ynyl)cyclopropyl ketone
CAS No.:1262862-88-3
Molecular Formula:C₂₁H₂₀O
Molecular Weight:288.389
Hs Code.:

Synonyms:phenyl 2-(5-phenylpent-4-ynyl)cyclopropyl ketone

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Chemical Property of phenyl 2-(5-phenylpent-4-ynyl)cyclopropyl ketone

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Technology Process of phenyl 2-(5-phenylpent-4-ynyl)cyclopropyl ketone

There total 1 articles about phenyl 2-(5-phenylpent-4-ynyl)cyclopropyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1774-47-6
trimethylsulfoxonium iodide

: (2E)-1,8-diphenyloct-2-en-7-yne-1-one

: 1262862-88-3
phenyl 2-(5-phenylpent-4-ynyl)cyclopropyl ketone

Guidance literature:: trimethylsulfoxonium iodide; With sodium hydride; In dimethyl sulfoxide;

(2E)-1,8-diphenyloct-2-en-7-yne-1-one; In dimethyl sulfoxide; at 0 - 20 ℃;
DOI:10.1021/ja107849y

Reference yield:

: 1262862-88-3
phenyl 2-(5-phenylpent-4-ynyl)cyclopropyl ketone

: phenyl (2S*,6aR*)-3-phenyl-1,2,4,5,6,6a-hexahydropentalen-2-yl ketone

Guidance literature:: With tris(bipyridine)ruthenium(II) dichloride hexahydrate; N,N,N,N,-tetramethylethylenediamine; magnesium sulfate; lanthanum(lll) triflate; In acetonitrile; for 16h; optical yield given as %de; diastereoselective reaction; Inert atmosphere; Visible light irradiation;
DOI:10.1021/ja107849y