C₃₂H₃₃ClN₆OS

Base Information

Chemical Name:C₃₂H₃₃ClN₆OS
CAS No.:1428759-18-5
Molecular Formula:C₃₂H₃₃ClN₆OS
Molecular Weight:585.173
Hs Code.:

C<sub>32</sub>H<sub>33</sub>ClN<sub>6</sub>OS

Synonyms:C₃₂H₃₃ClN₆OS

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Chemical Property of C₃₂H₃₃ClN₆OS

Chemical Property:

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Technology Process of C₃₂H₃₃ClN₆OS

There total 9 articles about C₃₂H₃₃ClN₆OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 943189-38-6
4-(1-ethyl-piperidin-4-yl)phenylamine

: 1428760-90-0
6-(2-chloro-4-(2-methyl-1,3-thiazol-5-yl)phenyl)-8-ethyl-2-(methylsulfinyl)pyrido[2,3-d]pyrimidin-7(8H)-one

: 1428759-18-5
C₃₂H₃₃ClN₆OS

Guidance literature:: at 100 - 120 ℃; for 1h;

Reference yield:

: 59748-90-2
4-Bromo-2-chloro-benzoic Acid

: 1428759-18-5
C₃₂H₃₃ClN₆OS

Guidance literature:: Multi-step reaction with 10 steps

1: 4-methyl-morpholine / tetrahydrofuran / 0.17 h / -15 °C

2: sodium tetrahydroborate; water / tetrahydrofuran / 1 h / -5 - 0 °C

3: phosphorus tribromide / 1,2-dichloro-ethane / 0.67 h / 0 - 10 °C

4: tetrabutyl-ammonium chloride / water; 1,2-dichloro-ethane / 4 h / 20 °C

5: sodium hydroxide / 4 h / Reflux

6: thionyl chloride / 1 h / Reflux

7: ISOPROPYLAMIDE; caesium carbonate / 2 h / 100 °C

8: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; ISOPROPYLAMIDE / 24 h / 110 °C / Sealed tube

9: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -5 - 20 °C

10: 1 h / 100 - 120 °C

With 4-methyl-morpholine; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; ISOPROPYLAMIDE; tetrabutyl-ammonium chloride; water; potassium acetate; phosphorus tribromide; caesium carbonate; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; 1,2-dichloro-ethane;

Reference yield:

: 185315-48-4
(4-bromo-2-chlorophenyl)methanol

: 1428759-18-5
C₃₂H₃₃ClN₆OS

Guidance literature:: Multi-step reaction with 8 steps

1: phosphorus tribromide / 1,2-dichloro-ethane / 0.67 h / 0 - 10 °C

2: tetrabutyl-ammonium chloride / water; 1,2-dichloro-ethane / 4 h / 20 °C

3: sodium hydroxide / 4 h / Reflux

4: thionyl chloride / 1 h / Reflux

5: ISOPROPYLAMIDE; caesium carbonate / 2 h / 100 °C

6: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium acetate; ISOPROPYLAMIDE / 24 h / 110 °C / Sealed tube

7: 3-chloro-benzenecarboperoxoic acid / dichloromethane / -5 - 20 °C

8: 1 h / 100 - 120 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; thionyl chloride; ISOPROPYLAMIDE; tetrabutyl-ammonium chloride; potassium acetate; phosphorus tribromide; caesium carbonate; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide; In dichloromethane; water; 1,2-dichloro-ethane;