(R)-5-((E)-2-pyrrolidin-3-ylvinyl)pyrimidine mono-di-p-anisoyl-D-tartarate

Base Information

Chemical Name:(R)-5-((E)-2-pyrrolidin-3-ylvinyl)pyrimidine mono-di-p-anisoyl-D-tartarate
CAS No.:1228391-45-4
Molecular Formula:C₁₀H₁₃N₃*C₂₀H₁₈O₁₀
Molecular Weight:593.59
Hs Code.:

Synonyms:(R)-5-((E)-2-pyrrolidin-3-ylvinyl)pyrimidine mono-di-p-anisoyl-D-tartarate

Suppliers and Price of (R)-5-((E)-2-pyrrolidin-3-ylvinyl)pyrimidine mono-di-p-anisoyl-D-tartarate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (R)-5-((E)-2-pyrrolidin-3-ylvinyl)pyrimidine mono-di-p-anisoyl-D-tartarate

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Technology Process of (R)-5-((E)-2-pyrrolidin-3-ylvinyl)pyrimidine mono-di-p-anisoyl-D-tartarate

There total 2 articles about (R)-5-((E)-2-pyrrolidin-3-ylvinyl)pyrimidine mono-di-p-anisoyl-D-tartarate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.4%

: 753015-44-0
(R)-5-((E)-2-pyrrolidin-3-ylvinyl)pyrimidine

: 50583-51-2,191605-10-4
O,O′-di-p-anisoyl-D-tartaric acid

: 1228391-45-4
(R)-5-((E)-2-pyrrolidin-3-ylvinyl)pyrimidine mono-di-p-anisoyl-D-tartarate

Guidance literature:: In ethanol; at 20 ℃; Heating;

Reference yield:

: 1228312-14-8
(R)-3-vinylpyrrolidine-1-carboxylic acid t-butyl ester

: 1228391-45-4
(R)-5-((E)-2-pyrrolidin-3-ylvinyl)pyrimidine mono-di-p-anisoyl-D-tartarate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium acetate / palladium diacetate; 1,1'-bis(diphenylphosphino)ferrocene / N,N-dimethyl acetamide / 16 h / 150 °C / Inert atmosphere

1.2: 1.5 h / 20 - 23 °C

2.1: ethanol / Heating

With sodium acetate; 1,1'-bis(diphenylphosphino)ferrocene; palladium diacetate; In ethanol; N,N-dimethyl acetamide;