(2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (E)-3-acetylpropenoate

Base Information

Chemical Name:(2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (E)-3-acetylpropenoate
CAS No.:1300748-90-6
Molecular Formula:C₁₈H₁₈N₂O₃
Molecular Weight:310.353
Hs Code.:

Synonyms:(2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (E)-3-acetylpropenoate

Suppliers and Price of (2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (E)-3-acetylpropenoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (E)-3-acetylpropenoate

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Technology Process of (2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (E)-3-acetylpropenoate

There total 4 articles about (2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (E)-3-acetylpropenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 2833-28-5
trans-4-oxo-2-pentenoic acid

: C₁₃H₁₄N₂O

: 1300748-90-6
(2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (E)-3-acetylpropenoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 30h; Inert atmosphere;
DOI:10.1039/c0ob00657b

Reference yield:

: methyl 3-(1-benzylimidazol-4-yl)-2-propenoate

: 1300748-90-6
(2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (E)-3-acetylpropenoate

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminium hydride

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 30 h / 20 °C / Inert atmosphere

With dmap; diisobutylaluminium hydride; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1039/c0ob00657b

Reference yield:

: 104-98-3
urocanic acid

: 1300748-90-6
(2E)-3-(1-benzyl-1H-imidazol-4-yl)-2-propenyl (E)-3-acetylpropenoate

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid; magnesium sulfate / Reflux

2: sodium hydride / tetrahydrofuran

3: diisobutylaluminium hydride

4: dmap; dicyclohexyl-carbodiimide / dichloromethane / 30 h / 20 °C / Inert atmosphere

With dmap; sulfuric acid; sodium hydride; diisobutylaluminium hydride; magnesium sulfate; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane; 1: Fischer esterification;
DOI:10.1039/c0ob00657b